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Ao Pan,Minghui Xie,Jianye Xia,Ju Chu,Ying-ping Zhuang 한국화학공학회 2018 Korean Journal of Chemical Engineering Vol.35 No.1
The influence of impeller structure on the mass transfer characteristics was studied with the steady-state method for gas-liquid volumetric mass transfer coefficient (kLa). The single-impeller configurations included eight impeller types (three radial flow impellers, four axial flow impellers and one mixed flow impeller), and the doubleimpeller included three configurations (RT+RT, RT+WHD, WHD+WHD). For single-impeller, the gas-liquid mass transfer rates of radial flow impellers were better than those of axial flow impellers under the same rotation speed and gas flow rate. The mass transfer performance (defined as the volumetric mass transfer coefficient per unit power input) of radial flow impellers were also better than that of axial flow impellers. With the same kLa value under a certain gas flow rate, the local bubble size distribution between radial flow impeller and axial flow impeller was similar. As for double impellers, RT+RT provided the highest mass transfer rate under certain rotation speed and gas flow rate, while WHD+WHD gave the highest values of gas-liquid mass transfer coefficient with the same power consumption.
Jiazhong Wu,Fanghui Liu,Hui Yang,Shijing Xu,Quan Xie,Minghui Zhang,TING CHEN,Guangxin Hu,Jinben Wang 한국공업화학회 2017 Journal of Industrial and Engineering Chemistry Vol.56 No.-
Low salinity effect has been in the center of attention as a cost-effective and environmentally friendlytechnique. Wettability alteration of the oil/brine/mica system appears to be the identified mechanism(s)to trigger the low salinity effect. While the effect of water chemistry and minerology on the wettability ofthe system has been extensively investigated, few studies have investigated the effect of specific functiongroups from crude oil on the system wettability, limiting the understanding of how specific functionalgroup contributes to the wettability. We thus experimentally measured the adhesion forces betweenmica surfaces and functional groups (e.g., C6H5–, CH3–, COOH–, and NH2–) in the presence of differentaqueous ionic solutions using chemical force microscopy (CFM). Moreover, to understand thecontribution of the structural force, the traditional Derjaguin–Landau–Verwey–Overbeek (DLVO) theorywas extended (denoted as EDLVO) tofit the force profiles using a Gauss model. Our results showed thatthe adhesion force between mica and functional groups in a decreasing order was –NH2> –COOH> –CH3> –C6H5. We also found that while DLVO forces strongly affected the tip-surface contact due to theinteractions among oil/brine/mica interfaces, the structural forces also played an important role in adistance of 1–20 nm due to the presence of H-bonds between COOH-terminated or NH2-terminated tipand mica surface. We therefore conclude that the structural force largely contributes to the adhesionforce due to the hydrophilicity or polarity of functional groups, and nucleophilic property (such as phenylgroup). Our results suggest that the polarity of the crude oil needs to be considered to screen a candidatereservoir for low salinity waterflooding projects.