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Hasanzadeh, Mohammad.,Shadjou, Nasrin.,Saghatforoush, Lotfali.,Khalilzadeh, Balal.,Kazeman, Isa. Korean Chemical Society 2009 Bulletin of the Korean Chemical Society Vol.30 No.12
Copper-dimethylglyoxime complex (CuDMG) modified Copper electrode (Cu/CuDMG) showed a catalytic activity towards cyclohexanol oxidation in NaOH solution. The modified electrode prepared by the dimethylglyoxime anodic deposition on Cu electrode in the solution contained 0.20 M $NH_4Cl\;+\;NH_4OH\;(pH\;9.50)\;and\;1\;{\times}\;10^{-4}$ M dimethylglyoxime. The modified electrode conditioned by potential recycling in a potential range of -900${\sim}$900 mV vs. Ag/AgCl by cyclic voltammetry in alkaline medium (1 M NaOH). The results show that the CuDMG film on the electrode behaves as an efficient catalyst for the electro-oxidation of cyclohexanol in alkaline medium via Cu (III) species formed on the electrode.
Mohammad. Hasanzadeh,Nasrin. Shadjou,Lotfali. saghatforoush,Balal. Khalilzadeh,Isa. Kazeman 대한화학회 2009 Bulletin of the Korean Chemical Society Vol.30 No.12
Copper-dimethylglyoxime complex (CuDMG) modified Copper electrode (Cu/CuDMG) showed a catalytic activity towards cyclohexanol oxidation in NaOH solution. The modified electrode prepared by the dimethylglyoxime anodic deposition on Cu electrode in the solution contained 0.20 M NH4Cl + NH4OH (pH 9.50) and 1 × 10-4 M dimethylglyoxime. The modified electrode conditioned by potential recycling in a potential range of ‒900 ~ 900 mV vs. Ag/AgCl by cyclic voltammetry in alkaline medium (1 M NaOH). The results show that the CuDMG film on the electrode behaves as an efficient catalyst for the electro-oxidation of cyclohexanol in alkaline medium via Cu (III) species formed on the electrode.