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Naveed Shahzad Ali,Abdul Ghaffar,Asif Ali Qaiser,Muhammad Ahmad,Khurram 한국고분자학회 2021 폴리머 Vol.45 No.1
The recovery of solvents from the extracted oils using conventional thermal separation processes i.e. distillation or evaporation is often an energy-intensive process. To provide an energy-efficient alternative, an organic solvent nanofiltration thin-film composite membrane was prepared by depositing a thin layer of polyaniline (PANI), a selective layer, via interfacial polymerization on a crosslinked polyimide (XPI), a base ultrafiltration support membrane, to provide selective transport of constituents of a miscella. The membrane was characterized by microscopic, spectroscopic, and thermal analysis. The evaluation of the separation performance was carried out by a dead-end stirred cell using three vegetable oils. For sunflower, corn, and castor oil/n-hexane mixtures, the membrane resulted in a % rejection of 50, 56, and -44, respectively. A comparison of mass flux and rejection of corn and castor oils suggests that the PANI/XPI membranes showed a strong ion-exchange behavior significantly recognizing charge macromolecules due to the presence of charged emeraldine PANI.
Irfana Moideen Kolangare,Arun Mohan Isloor,Asif Ali Qaiser,Ahmed Fauzi Ismail,Mohd Sohaimi Abdullah 한국화학공학회 2018 Korean Journal of Chemical Engineering Vol.35 No.6
This work deals with a simple and eco-friendly approach for the development of ultrafiltration membranes for the separation of environmentally hazardous substances from the water source. Polysulfone and sulfonated polyphenylsulfone blend ultrafiltration membranes were fabricated by the non-solvent induced phase inversion technique. Prepared membranes were characterized for their morphology, hydrophilicity, porosity, filtration and antifouling properties. The blend membranes with 15 wt% of sPPSU demonstrated the best performance with water flux of 190.33 Lm2h1 and flux recovery ratio of 86.56%. The effect of aq. glycine betaine (GB) coagulation bath on the membrane property and performance was studied and compared with commonly used additives such as NaCl and NMP. The GB in coagulation bath exhibited better flux and performance with protein rejection of 66.3%, 74.0% and 91.2% for trypsin, pepsin, and bovine serum albumin, respectively, and heavy metal rejection of 75.2% and 87.6% for polymer enhanced ultrafiltration of Cd2+ and Pb2+ ions, respectively.