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섬유상 $BaTiO_3$의 분말 직경에 따른 흡진 특성
서용교,야나기다히로아끼,Seo, Yong-Gyo 한국재료학회 1994 한국재료학회지 Vol.4 No.1
Recently, sound and mechanical vibration are becoming important problems in our life. In the present study, the measurement of vibration absorption characteristics of barium titanate ceramics and the investigation of its relationship to microstructures were carried out. The barium titanate ceramics is expected to be better vibration absorption material owing to its chemical and physical stability than other conventional vibration absorbers like glasswool board. Barium titanate ceramics were prepared by sintering fiberous $BaTiO_{3}$ crystallites in order to enhance the vibration absorption characteristics. The fiberous $BaTiO_{3}$ ceramics were prepared through the ionic exchange after the preparation of fiberous $K_2Ti_4O_9$ with 0.2$\mu\textrm{m}$, 1.2$\mu\textrm{m}$, 2.0$\mu\textrm{m}$, diameter length by KDC method. The fiberous crystallites were oriented in a plane perpendicular to the press direction and sintered. The investigation of the grain diameters of the sintered ceramics, equivalent factor, electromechanical coupling factor($k_1$), and the generated voltage(V) shows that the grain's diameter decreases with the increase of the diameter of the used fiberous crystallites. The vibration absorption increases the crystallites' diameter. That means that the vibration absorption increases with the internal friction of grain boundary. Which was identified by the investigation of the equivallent circuit. 최근 중요하게 된 진동 흡수를 위해서 $BaTiO_{3}$ 세라믹의 흡진 특성을 측정하고 미세구조와의 연관을 조사했다.$BaTiO_{3}$ 세라믹은 비교적 물리적 화학적으로 안정하여 좋은 흡진재로 기대된다.BaTiO$_{3}$ 세라믹은 흡진 특성을 강화시키기 위해서 섬유상 분말을 소결하여 만들었다. KDC법으로 직경이 0.2$\mu\textrm{m}$, 1.2$\mu\textrm{m}$, 2.0$\mu\textrm{m}$인 각각 다른 섬유상 $K_2Ti_4O_9$을 만들고 이온교환해서 섬유상 $BaTiO_{3}$ 을 만들었다. 면상으로 배향시킨 소결체의 흡진 특성과 전기적 물성을 조사하여 미세구조와 의 관계를 밝혔다. 소결체의 입경과 등가회로, 전기기계합계수($K_{t}$), 발생 전압(V)을 조사한 결과, 사용한 섬유의 직경이 클수록 소결체의 입경은 작아졌다. 따라서 입계가 많아졌다. 흡진 특성은 입계가 많을수록 커진다. 즉 입계의 내무마찰이 클수록 흡진률은 커지며 이때의 내부마찰은 등가회로를 조사함으로써 확인되었다.
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섬유상 분말로 제조된 배향성을 가진 $BaTiO_3$ 세라믹
서용교,야나기다히로아끼 한국세라믹학회 1993 한국세라믹학회지 Vol.30 No.12
When looked upon as a polycrystalline, ceramics have two basic differences from a single crystal. One is that there exist grain boundaries, the other is that the crystal axes of each small crystal are arranged in random directions. But the crystal axes fo small crystals which compose ceramics may be made to have the tendency of being arranged in a specific direction. This is called that the crystal axes are oriented. The degree of the direction arrangement of the crystal axes is called orientation. In order to orient the crystal axes effectively, the fiberous barium titanates were made through KDC method and the ion exchange method. And then they were arranged through pressing, doctor blade, and syringe. As the result of Lotgering evaluation, the sample oriented through syringe showed the highest orientation. After sintering, though the most particles that had been fiberous shaped became global shape viewed through SEM, the orientation of the crystals was reinforced by means of sintering.
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