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      • KCI등재

        Investigation on High Temperature Mechanical Behaviors of TiC-γ′ Reinforced Ni Composite

        Wenqiang Hu,Zhenying Huang,Qun Yu,Yuanbo Wang,Yidan Jiao,Yang Zhou,Hongxiang Zhai 대한금속·재료학회 2021 METALS AND MATERIALS International Vol.27 No.8

        A duplex TiC and γ′-Ni3(Al,Ti) reinforced nickel composite was fabricated through hot-press sintering a 30 vol% Ti2AlC–Nimixtures followed by thermal treatment method. Detailed microstructural detection was performed by adopting the routeof high-resolution transmission electron microscopy. In situ generated submicron TiC particulate and nanosized L12-γ′were homogeneously distributed in a fcc γ-Ni matrix. The high temperature tensile and compression behaviors of the TiC-γ′/Ni composites were evaluated in the temperature range of 25–800 °C. The results indicated that ultimate tensile andcompression properties exhibited the dependence of temperatures. The tensile properties of the composite determined at600 °C was 945 MPa, decreasing by 28.1% and 23.0% for elongation, compared to those of measured at room temperature(UTS = 1305 MPa, elongation = 5.35%). However, the yield strength exhibited the temperature independent until to 600 °C. The yield strength of the TiC-γ′/Ni composite are comparable with conventional superalloy under 600 °C, proving that TiCand γ′ particles constitute efficient reinforcements for Ni matrix according to thermal expansion dislocations strengthening,load-transfer and coherent strengthening mechanisms. The monotonic temperature dependence of yield strength at600–800 °C indicates that plastic deformation of TiC-γ′/Ni composite follows the thermally activated mechanism. TheTiC-γ′/Ni composite exhibited superior mechanical properties both at room and high temperatures, which can be ascribedto the synergistic strengthening effect in term of dislocation density, Orowan, coherent and atomic ordering strengtheningmechanisms. The present work reveals the deformation behaviors of in situ TiC-γ′/Ni composite from room to high temperatures,which is critical to predict the failure and thereby optimize the microstructure to further enhance the high temperatureproperties of TiC-γ′/Ni composite.

      • KCI등재

        Thermal Shock Behavior of a Novel TiCx–Ni3(Al,Ti)/Ni Functionally Graded Composite

        Qun Yu,Zhenying Huang,Guangming Zheng,Wenqiang Hu,Cong Lei,Yuanbo Wang,Yidan Jiao,Hongxiang Zhai 대한금속·재료학회 2021 METALS AND MATERIALS International Vol.27 No.12

        This paper focuses on the study of thermal shock behaviors of a novel TiCx–Ni3(Al,Ti)/Ni functionally graded material (FGM)fabricated from Ti3AlC2and Ni powders. Thermal shock resistance of resulted FGM was conducted by water quenching atdifferent temperatures, mechanical properties and microstructures after thermal shocks were correspondingly determined andcharacterized. The microstructure of the FGM after thermal shocks shows no cracks of instability failure between the transitionzones, and the reinforcement phases were closely combined with the matrix. Meanwhile, compared with the strengthof 1329 MPa without thermal shock, when the temperature of the thermal shock reached 800 °C and 1000 °C respectively,with 10 repeated heat-water quench cycles, the residual flexural strength of FGM decreased slightly, but it could still reach1100 MPa. Notably, the strength can still maintain at 843 MPa after 10 cycles of thermal shock at 1200 °C. Such excellentthermal shock performance may be the result of the good interfacial bonding and the special gradient structure, the oxidationlayer also plays a protective role.

      • KCI등재

        Microstructural and Mechanical Properties of TiCX–Ni3(Al,Ti)/Ni Functionally Graded Composites Fabricated from Ti3AlC2 and Ni Powders

        Guangming Zheng,Zhenying Huang,Qun Yu,Wenqiang Hu,Xingyang Qiu,A. Lixia,Yuanbo Wang,Yidan Jiao,Yang Zhou,Hongxiang Zhai 대한금속·재료학회 2020 METALS AND MATERIALS International Vol.26 No.6

        In this paper, a novel type of functionally graded material (FGM) was successfully fabricated from pure Ni and Ti3AlC2powder mixtures by hot-press sintering route at 1200 °C and 17 MPa. In each layer, Ti3AlC2particles transformed into TiCxphase, while the additional Al–Ti atoms decomposed from Ti3AlC2diffused into the Ni matrix, giving rise to the formationof γ′-Ni3(Al,Ti). Part of the submicron TiCxand Ni3(Al,Ti) particles were uniformly distributed in the Ni matrix, whilesome of the TiCxmaintained the original Ti3AlC2plate-like morphology. Both TiCxand Ni3(Al,Ti) content decreased from60Ti3AlC2/Ni layer to 10Ti3AlC2/Ni layer in a stepwise manner was fabricated. The microstructural analysis indicatesthat no cracks, delamination and step-type abrupt changes occured in the graded layer of the manufactured FGM. Flexuralstrength and Vickers hardness enhanced with the increasing Ti3AlC2content except for fracture strain and toughness. Theoverall fracture toughness and the flexural strength of FGM can reach 21.76 MPa m1/2 and 1329 ± 34 MPa, respectively. Theprepared FGM, herein, with a hard ceramic surface on one side to resist local plastic deformation, and a ductile metallicsurface on the other side to provide toughness.

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