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Ziqiang Xu,Jinchen Chen,Mengqiang Wu,Cheng Chen,Yaochen Song,Yuesheng Wang 대한금속·재료학회 2019 ELECTRONIC MATERIALS LETTERS Vol.15 No.4
Hard carbon is deemed to be a most promising anode materials for sodium—ion batteries (SIBs), while, the issues of lowcapacity and low initial coulombic efficiency still exist limiting the development of SIBs. Although high temperature carbonizationof biomass materials under nitrogen or argon atmosphere is a common method for preparation of hard carbon,there are few reports about the effects of different protective atmospheres on propriety of hard carbon. In this article, hornet’snest (HN) is used to prepare hard carbon under nitrogen and argon. At a suitable carbonization temperature (1200 °C and1400 °C), the hard carbon under argon possesses lower specific surface area (25–50 cm−3 g−1), but higher initial coulombefficiency (4–6%) and higher capacity retention (3–6%). Thus, it is inferred that high—performance hard carbon can beobtained under argon atmosphere. Our research about the effect of sintering atmosphere on material properties is expectedto provide a reference for the synthetization of hard carbon by high temperature carbonization.
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