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Narasinga Rao Palepu,Werner Kaminsky,Mohan Rao Kollipara 대한화학회 2017 Bulletin of the Korean Chemical Society Vol.38 No.1
A series of Cp*Rh and Cp*Ir complexes of picolinic hydrazine ligand are synthesized and characterized. Picolinic hydrazine has yielded only dinuclear complexes in the case of rhodium metal whereas both mono and dinuclear complexes with iridium metal. Iridium complexes are formed as quaternary salts by the migration of the N–H proton onto the adjacent amine group of the hydrazine after binding to the metal. Picolinic hydrazine acts as nitrogen and oxygen donor ligand in the form of bi and tetradentate bonding modes.