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AlN matrix composites fabricated by the spark plasma sintering –reactive synthesis method
Tiekun Jia,Weimin Wang,Zhengyi Fu,Hao Wang 한양대학교 세라믹연구소 2009 Journal of Ceramic Processing Research Vol.10 No.6
A mixture of Al and BN powders was adopted to synthesize AlN matrix composites using the spark plasma sintering-reactive (SPS) synthesis method. The crystalline phases of sintered samples were characterized by X-ray diffraction (XRD). Scanning electron microscope (SEM) and transmission electron microscope (TEM) images of the microstructure revealed that the BN phase was homogeneously distributed in the matrix of synthesized AlN. The effect of sintering temperature on the microstructure and properties of sintered samples was investigated. The results showed that densification of sintered samples was improved and the thermal conductivity exhibited a significant increase with an increase of the sintering temperature. A mixture of Al and BN powders was adopted to synthesize AlN matrix composites using the spark plasma sintering-reactive (SPS) synthesis method. The crystalline phases of sintered samples were characterized by X-ray diffraction (XRD). Scanning electron microscope (SEM) and transmission electron microscope (TEM) images of the microstructure revealed that the BN phase was homogeneously distributed in the matrix of synthesized AlN. The effect of sintering temperature on the microstructure and properties of sintered samples was investigated. The results showed that densification of sintered samples was improved and the thermal conductivity exhibited a significant increase with an increase of the sintering temperature.
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