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Determination of Thermo-Electrical Properties in Sn Based Alloys
Sezen Aksöz,Yavuz Ocak,Kâzlm Keslioslu,Necmettin Mara ll 대한금속·재료학회 2010 METALS AND MATERIALS International Vol.16 No.3
The variation of thermal conductivity of solid phase versus temperature for Sn-21 wt.% Bi, Sn-25 wt.% In and Sn-35 wt.% In-26 wt.% Bi alloys were measured with a radial heat flow apparatus. From the graphs of thermal conductivity versus temperature, the thermal conductivity of the solid phases at their melting temperatures and the thermal temperature coefficients for the same alloys were obtained. The ratios of thermal conductivity of liquid phase to solid phase for the same materials were measured with a Bridgman type directional solidification apparatus. The variations of electrical conductivity of solid phases versus temperature for the same alloys were determined from the Wiedemann-Franz law by using the measured values of thermal conductivity. From the graphs of electrical conductivity versus temperature, the electrical temperature coefficients for the same alloys were also determined. According to present experimental results it can be concluded that the thermal and electrical conductivity of Sn based alloys depend on the thermal and electrical conductivity of the alloying elements. If the thermal and electrical conductivity of the alloying elements are lower than the thermal conductivity of Sn, the thermal conductivity of Sn based alloys decreases, whereas, otherwise,it increases.
Experimental Determination of Interfacial Energies for Solid Sn in Equilibrium with Sn-Mg-Zn Liquid
Yemliha Altıntas,Esra Öztürk,Sezen Aksöz,Kâzım Keşlioğlu,Necmettin Maraşlı 대한금속·재료학회 2015 METALS AND MATERIALS International Vol.21 No.2
The equilibrated grain boundary groove shapes of solid Sn in equilibrium with Sn-Mg-Zn liquid were observedfrom a quenched sample by using a radial heat flow apparatus. The Gibbs-Thomson coefficient, solid-liquidinterfacial energy and grain boundary energy of solid Sn were determined from the observed grain boundarygroove shapes. The thermal conductivity of the eutectic solid phase for Sn-8.12 at% Mg-4.97 at% Zn alloy and thethermal conductivity ratio of the liquid phase to the solid phase for Sn-8.12 at% Mg-4.97 at% Zn alloy at eutectictemperature were also measured with a radial heat flow apparatus and a Bridgman-type growth apparatus,respectively. The Gibbs-Thomson coefficient, solid-liquid interfacial energy and grain boundary energy of solidSn in equilibrium with Sn-Mg-Zn liquid were determined to be (8.3 ± 0.6)×10-8 Km, (118.5 ± 14.2)×10-3 Jm-2and (225.1 ± 29.3)×10-3 J m-2 respectively from observed grain boundary groove shapes. A comparison ofpresent results for solid Sn in the Sn-8.12 at% Mg-4.97 at% Zn alloy with the results obtained in previous worksfor similar solid Sn in equilibrium with different binary or ternary liquid was made.