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- 저자 : Rashidi Hamed (검색결과 4 건)
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Hamed Rashidi,Ahmad Shariati,Mohammad Reza Khosravi Nikou,Touba Hamoule 한국화학공학회 2016 Korean Journal of Chemical Engineering Vol.33 No.8
MSU-S catalyst, assembled from ZSM-5 zeolite seed (MFI), was synthesized with silica to alumina ratio 55 and characterized by XRD, NH3-TPD, BET and FT-IR techniques. It was tested in a vertical fixed bed reactor for selective production of light olefins from methanol (MTO) at temperatures of 400, 450 and 500 oC and WHSV of 1, 5 and 25 h−1. After thorough investigation, it was found that WHSV=5 h−1 and temperature of 500 oC are the optimum conditions for maximum light olefin yield, which was 52% with propylene to ethylene ratio of 4.57. Acidity of MSU-S was promoted by incorporation of phosphotungusticacid (HPW) and a direct method to reach high HPW dispersion and thermal stability. Maximum light olefin yield was observed over HPW-MSU-S at the optimum reaction conditions to be nearly 60% with propylene to ethylene ratio of 4.3.
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Carbon dioxide absorption by Ammonia-promoted aqueous triethanolamine solution in a packed bed
Rashidi Hamed,Azimi Hossein,Rasouli Parvaneh 한국화학공학회 2023 Korean Journal of Chemical Engineering Vol.40 No.9
CO2 absorption by ammonia added triethanolamine aqueous solution as a promoter was investigated in terms of absorption percentage (AP), overall volumetric mass transfer coefficient (KGae), and molar flux (NA) in a packed column. Three variables of ammonia concentration (0–5 wt%), Triethanolamine concentration (10–30 wt%), and gas flow rate (1,500–2,500 ml/min) were considered as significant variables in absorption performance. Effect of these variables and their interactions were inspected using the three level factorial response-surface method. Statistical analysis of the results showed that an ammonia concentration with 72.99%, 71.83, and 81.12% has the greatest effect on AP%, NA, and KGae, respectively. Then, gas flow rate with 5.27% and 3.90%, had a great effect on AP% and KGae, respectively. Finally, the optimal operating conditions were determined to maximize the responses. Under optimal operating conditions, the maximum values for AP%, KGae, and NA were 98.94%, 0.202 kmol/h·m3·kPa, and 3.901 kmol/m2·h, respectively. Thus, adding ammonia to triethanolamine considerably improves the mass transfer performance of solvent.
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Masoud Rahimi,Peyvand Valeh-e-Sheyda,Hamed Rashidi 한국화학공학회 2017 Korean Journal of Chemical Engineering Vol.34 No.11
The paper deals with the development and optimization of curcumin nanosuspension by solvent/anti-solvent precipitation method in a microfluidic platform. A three-level Box-Behnken design was applied as an optimizing technique to investigate the effect of three independent operating variables, namely, volume ratios of anti-solvent to solvent, flow rate of drug solution, and curcumin concentration on the preferred response. In presence of PVP as the stabilizer, a nano-curcumin suspension was obtained in the range of 62-335nm. Analysis of variance showed that the variables with the highest effect were the linear effects of the anti-solvent to solvent ratio, and its corresponding squared term. Applying response surface methodology, curcumin nanosuspension with average size of 63.12 nm can be obtained under optimum condition As: S=15, solvent flow rate of 1.0mL/min and curcumin ethanolic concentration of 5.0mg/mL. The prepared nanoparticles were further characterized by infrared spectroscopy, scanning electron microscopy, and X-ray diffraction tests.
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ALI AYATI,ALI AHMADPOUR,FATEMEH F. BAMOHARRAM,MAJID M. HERAVI,HAMED RASHIDI 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2012 NANO Vol.7 No.1
Preparation of gold nanoparticles by chemical reduction method using Preyssler heteropolyacid was investigated. The experimental conditions have been optimized using Taguchi robust design method with L9 orthogonal array. Particle size of the gold nanoparticles was considered as the property in the optimization. Amounts of Preyssler heteropolyacid, pH and irradiation time were selected as the main parameters. The result of Taguchi analysis has shown that in this process, the preyssler acid amount is the most influencing parameter on the size of gold nanoparticle. Also, the effects of different parameters are in order to: Preyssler acid amount > pH > irradiation time (negligible). This method showed that decreasing Preyssler amount and increasing pH of solution lead to formation of smaller nanoparticles. Finally, the prepared nanoparticles at optimum condition with a size of about 6.42 were characterized by using Dynamic Light Scattering (DLS) method, transmission electron microscopy (TEM), and UV-Vis spectroscopy.
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