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- 검색키워드
- 저자 : Rahman Mukhlis A. (검색결과 3 건)
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Nizar Mu’ammar Mahpoz,Norfazliana Abdullah,Mohamad Zahir Mohd Pauzi,Mukhlis A. Rahman,Khairul Hamimah Abas,Azian Abd Aziz,Mohd Hafiz Dzarfan Othman,Juhana Jaafar,Ahmad Fauzi Ismail 한국화학공학회 2019 Korean Journal of Chemical Engineering Vol.36 No.3
This work describes the development of zeolitic imidazolate framework-8 (ZIF-8) membranes on modified alumina hollow fiber for desalination by forward osmosis. Effects of different seeds (ZnO, NiO and PDA) and sodium formate on in-situ deposition of ZIF-8 were studied in relation to the membrane’s morphology and performance. XRD result shows that ZIF-8 was successfully synthesized in the presence of sodium formate. FESEM images showed PDA modified support was unsuccessful in producing well defined and dense ZIF-8 membrane layer even after another ZIF-8 re-deposition due to its minimal amount. The NiO modified support was also found unsuccessful, as ZIF-8 crystals were formed in clusters. On the contrary, dense ZIF-8 membrane was successfully prepared on ZnO modified support with SF-1 synthesis solution producing bigger ZIF-8 crystal and thinner ZIF-8 membrane than as of SF-2. Water flux performance in forward osmosis showed that NiO/ZIF-8, PDA/ZIF-8 and PDA/ZIF-8 (re-deposition) membranes gave negative water fluxes of 50 kg/m2·h, 5.2 kg/m2·h and 1.7 kg/m2·h with reverse solutes of 42.66 mol/m2·h, 27.42mol/m2·h and 3.22 mol/m2·h, respectively, indicating the solute from draw solution diffused into the feed solution. However, ZIF-8 membrane prepared using SF with molar ratio of 1, on the ZnO modified support had a water flux of 13.3 kg/m2·h, reverse solute of 0.95 kg/m2·h and salt rejection of 52.1%. When the SF ratio was increased to 2, the ZIF-8 membranes showed a water flux of 12.5 kg/m2·h, reverse solute of 1.64 kg/m2·h and salt rejection of 54.9%. The moderate salt rejection could be associated with defects in the ZIF-8 membranes due to poor grain boundaries.
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Sohaimi Khairunissa Syairah Ahmad,Jaafar Juhana,Dharma Hadi Nugraha Cipta,Samuel Ojo,Ismail A. F.,Othman M. H. D.,Rahman Mukhlis A.,Aziz F.,Salleh W. N. W. 한국화학공학회 2024 Korean Journal of Chemical Engineering Vol.41 No.3
In this research, an innovative Z-scheme vanadium pentoxide (V 2 O 5 )/graphitic carbon nitride (g-C 3 N 4 ) photocatalyst was synthesised using a facile thermal treatment method, and its photodegradation performance and physicochemical properties were evaluated. The heterostructure provided high Brunauer–Emmett–Teller surface area and pore volume, which encouraged charge carrier separation and transfer, as well as supplied abundant micro-mesoporous structures and active sites for photocatalytic redox reactions. The successful incorporation of V 2 O 5 between g-C 3 N 4 layers can be proven by proposing the synthesis mechanism, as well as conducting morphology, crystal structure, elemental, and chemical analysis through scanning electron microscopy, X-ray diff raction, energy dispersive X-ray spectroscopy, and X-ray photoelectron spectroscopy, respectively. Using these combined photocatalysts, ciprofl oxacin (CIP) was successfully degraded up to 90.17% removal effi ciency in the visible-light spectrum. The superior photocatalytic activity of g-C 3 N 4 composite over V 2 O 5 is primarily due to its increased light absorption capacity, as well as increased surface area, pore size, and volume, eff ective charge transfer, and optimal band alignment between g-C 3 N 4 and V 2 O 5 . This research provides a signifi cant future perspective for the utilisation of Z-scheme V 2 O 5 /g-C 3 N 4 heterojunction photocatalyst for water treatment, especially those involving endocrine-disrupting compounds and antibiotics like CIP.
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Mohd Ridhwan Adam,Mohd Hafiz Dzarfan Othman,Siti Hamimah Sheikh Abdul Kadir,Muthia Elma,Tonni Agustiono Kurniawan,Ahmad Fauzi Ismail,Mohd Hafiz Puteh,Azeman Mustafa,Mukhlis A. Rahman,Juhana Jaafar,Hud 한국화학공학회 2021 Korean Journal of Chemical Engineering Vol.38 No.4
This work investigates the effectiveness of ammoniacal nitrogen (NH4 +-N) removal from contaminated water by adsorptive hollow fiber ceramic membrane (HFCM) derived from naturally made clinoptilolite. The technological value of this work is the simple mechanism of the adsorptive HFCM in removing gaseous ammonia in water by combining adsorption and separation. To test the technical feasibility of this proposed technology, clinoptilolite HFCM was fabricated via phase inversion-based extrusion/sintering technique and characterized by SEM and water permeation flux. The produced HFCM corresponds to the desired morphology of the asymmetric structure (dense and void formations) with outstanding adsorption performance of NH4 +-N. The effects of the HFCM’s operational parameters on its removal are examined in terms of membrane dosage and isothermal studies. The adsorption isotherm behavior exhibited that the adsorption process fitted the Freundlich isotherm model with outstanding removal performance even at trace concentration of ammonia. The low amount used by HFCM (4.75×104m2) resulted in over 96% ammonia removal, indicating a low cost of adsorption process. The regeneration of saturated HFCM suggests an outstanding recovery of the HFCM for its subsequent use for NH4 +-N removal. This study also reveals the potential of adsorptive HFCM as a simple and cost-effective technology for ammonia removal from wastewater.
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