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Paramita Bhattacharjee,Probir Kumar Ghosh 한국화학공학회 2016 Korean Journal of Chemical Engineering Vol.33 No.5
Methyl eugenol-rich extracts from dried tuberose flowers (Polianthes tuberosa L.) of Calcutta single variety were obtained using supercritical carbon dioxide (SC-CO2) extraction. The optimized conditions for highest yield of methyl eugenol were 50 oC, 300 bar, 135 min with 1 L min−1 flow rate of gaseous CO2. Solubilities of methyl eugenol under different SC-CO2 extraction conditions were evaluated by Hildebrand solubility parameter and Chrastil equation. The extraction curve of methyl eugenol followed plug flow model. Steady state extraction occurred up to 100min, followed by unsteady state. Release of methyl eugenol from tuberose flowers followed first-order kinetics (Peppas model) and non-Fickian diffusion. Packed bed characterization was carried out using dimensionless numbers of mass transfer, considering steady and unsteady states of extraction. These findings could be used in the development of the pilot plant and commercial scale extraction of methyl eugenol from floral matrices.
Sayani Pal,Paramita Bhattacharjee 한국식품과학회 2017 Food Science and Biotechnology Vol.26 No.6
Yellow maize kernels were subjected to supercritical carbon dioxide (SC-CO2) extraction to obtain a lutein-rich extract with potential nutraceutical properties. SC-CO2 extraction parameters (pressure and temperature) were optimized by employing a full-factorial (32) design of experiments and response surface methodology, based on yield of lutein, antioxidant activity, andx-6/x-3 fatty acid ratio of the extracts. A Chrastil equation was also developed for predicting the solubility of lutein in SC-CO2 under different extraction conditions. The optimized extraction condition was obtained at 500 bar, 70 C for 90 min, at which the extract was found to possess a unique combination of the highest lutein yield (275.00 ± 3.50 lg/g of dry weight), along with a well-balanced x-6/x-3 fatty acid ratio (3:1). Moreover, the total phenol content and antioxidant activity were also found to be the highest at this condition. This lutein-rich extract is a promising nutraceutical or dietary supplement in the food industry.