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RISS 인기검색어
- 검색키워드
- 저자 : I. Juárez-Ramírez (검색결과 3 건)
- 무료
- 기관 내 무료
- 유료
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Particle size effect of LiAlSiO₄on the thermal expansion of SiC porous materials
I. Juárez-Ramírez,K. Matsumaru,K. Ishizaki,L.M. Torres-Martínez 한양대학교 세라믹연구소 2008 Journal of Ceramic Processing Research Vol.9 No.5
This paper reports the effect of the particle size of LiAlSiO4 on the thermal expansion and Young’s modulus of low thermal expansion (LTE) coefficient of porous materials using silicon carbide (SiC), vitrified bonding material (VBM) and lithium aluminum silicate (LiAlSiO4) at 850 oC. According to the XRD results, there is no reaction between the raw materials during the sintering process. SEM analysis revealed the presence of an internal porous structure with a pore size less than 4 micrometers. It was found that decreasing the particle size of LiAlSiO4 by almost 4 times reduces the porosity, keeping a low thermal expansion coefficient, but the Young’s modulus increases 50%. This paper reports the effect of the particle size of LiAlSiO4 on the thermal expansion and Young’s modulus of low thermal expansion (LTE) coefficient of porous materials using silicon carbide (SiC), vitrified bonding material (VBM) and lithium aluminum silicate (LiAlSiO4) at 850 oC. According to the XRD results, there is no reaction between the raw materials during the sintering process. SEM analysis revealed the presence of an internal porous structure with a pore size less than 4 micrometers. It was found that decreasing the particle size of LiAlSiO4 by almost 4 times reduces the porosity, keeping a low thermal expansion coefficient, but the Young’s modulus increases 50%.
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Silver nanoparticles incorporated into Na₂Ti6O13 microfibers
V. Rodríguez-González,I. Juárez-Ramírez,R. Zanella,M.E. Zarazúa,L.M. Torres-Martínez 한양대학교 세라믹연구소 2008 Journal of Ceramic Processing Research Vol.9 No.6
This research is concerned with novel semiconductor composites of sodium hexatitanate oxide (Na2Ti6O13), and silver metallic nanoparticles. The Na2Ti6O13 was prepared by two methods, a sol-gel process and a solid state reaction. The silver nanoparticles were incorporated into the titanate by a deposition-precipitation technique, using NaOH as precipitation agent in the dark. Ag/Na2Ti6O13 microfibers were obtained by the sol-gel method, meanwhile octagonal microbar agglomerates were the product of the solid state reaction. The SEM-TEM observations showed silver particles with a nanometric size (5-7 nm); and fibrillar structures in the sol-gel sodium titanates. The UV-Vis-RD spectroscopy showed a blue shift Eg from 3.3 to 3.4 nm; and a plasmon surface resonance in the visible region. These materials are proposed as potential photocatalysts for contaminated water purification. This research is concerned with novel semiconductor composites of sodium hexatitanate oxide (Na2Ti6O13), and silver metallic nanoparticles. The Na2Ti6O13 was prepared by two methods, a sol-gel process and a solid state reaction. The silver nanoparticles were incorporated into the titanate by a deposition-precipitation technique, using NaOH as precipitation agent in the dark. Ag/Na2Ti6O13 microfibers were obtained by the sol-gel method, meanwhile octagonal microbar agglomerates were the product of the solid state reaction. The SEM-TEM observations showed silver particles with a nanometric size (5-7 nm); and fibrillar structures in the sol-gel sodium titanates. The UV-Vis-RD spectroscopy showed a blue shift Eg from 3.3 to 3.4 nm; and a plasmon surface resonance in the visible region. These materials are proposed as potential photocatalysts for contaminated water purification.
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A. Martínez-de la Cruz,S. Obregón Alfaro,Leticia M. Torres-Martínez,I. Juárez Ramírez 한양대학교 세라믹연구소 2008 Journal of Ceramic Processing Research Vol.9 No.5
Bismuth tungstate Bi2W2O9 has been synthesized using diethylenetriaminepentaacetic acid (H5DTPA), an organic chelating agent of metals in an aqueous solution. The formation of the oxide was followed through characterization techniques such as XRD, TGA/DTA, and SEM. The optimum temperature to decompose the organic matrix and to form Bi2W2O9 was determined to be around 720 oC. Below this temperature, Bi2W2O9 was formed with a high content of Bi2WO6. At 720 oC particles of the Bi2W2O9 with a surface area four times higher than that obtained by a solid-state reaction were obtained. The oxide was tested as a photocatalyst on the degradation of aqueous solutions of rhodamine B under VIS radiation. The photodegradation of the dye followed a kinetic first order with an apparent constant, k = 2.8 × 10−3 minute−1and t1/2= 247 minutes for an aqueous solution of 5 mg l−1 of rhodamine B. Bismuth tungstate Bi2W2O9 has been synthesized using diethylenetriaminepentaacetic acid (H5DTPA), an organic chelating agent of metals in an aqueous solution. The formation of the oxide was followed through characterization techniques such as XRD, TGA/DTA, and SEM. The optimum temperature to decompose the organic matrix and to form Bi2W2O9 was determined to be around 720 oC. Below this temperature, Bi2W2O9 was formed with a high content of Bi2WO6. At 720 oC particles of the Bi2W2O9 with a surface area four times higher than that obtained by a solid-state reaction were obtained. The oxide was tested as a photocatalyst on the degradation of aqueous solutions of rhodamine B under VIS radiation. The photodegradation of the dye followed a kinetic first order with an apparent constant, k = 2.8 × 10−3 minute−1and t1/2= 247 minutes for an aqueous solution of 5 mg l−1 of rhodamine B.
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