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- 저자 : Albert C. Kneiss (검색결과 1 건)
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Characterisation of Melt Spun Ni-Ti Shape Memory Ribbons’ Microstructure
Kambiz Mehrabi,Mihael Brunˇcko,Albert C. Kneiss,Miodrag ˇColiˇc,Dragoslav Stamenkovic,Janko Ferˇcec,Ivan Anžel,Rebeka Rudolf 대한금속·재료학회 2012 METALS AND MATERIALS International Vol.18 No.3
NiTi alloys are the most technologically important medical Shape Memory Alloys in a wide range of applications used in Orthopaedics, Neurology, Cardiology and interventional Radiology as guide-wires,self-expandable stents, stent grafts, inferior vena cava filters and clinical instruments. This paper discusses the use of rapid solidification by the melt spinning method for the preparation of thin NiTi ribbons for medical uses. Generally, the application of rapid solidification via melt-spinning can change the micro-structure drastically, which improves ductility and shape memory characteristics and leads to samples with small dimensions. As the increase in the wheel speed led to a reduced ribbon thickness, the cooling rate increased and, therefore, the martensitic substructure became finer. Furthermore, no transition from the crystalline phase to the amorphous phase was obtained by increasing the cooling rate, even at a wheel speed of 30 m/s. Specimens for our metallographic investigation were cut from the longitudinal cross sec-tions of melt-spun ribbons. Conventional TEM studies were carried out with an acceleration voltage of 120 kV. Additionally, the chemical composition of the samples was examined with a TEM equipped with an EDX analyser. The crystallographic structure was determined using Bragg-Brentano x-ray diffraction with Cu-Kα radiation at room temperature.
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