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RISS 인기검색어
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- 저자 : A. Valadez-González (검색결과 3 건)
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Javier I. Cauich‑Cupul,Pedro J. Herrera‑Franco,Edgar García‑Hernández,Veronica Moreno‑Chulim,Alex Valadez‑González 한국탄소학회 2019 Carbon Letters Vol.29 No.4
A two-level full factorial design 22 with three replications was employed to assess the effect of the incorporation of PSF into the epoxy matrix and the surface treatment of carbon fibers on the work of adhesion (WA) and the interfacial shear strength (IFSS) of carbon fiber–epoxy composites. The IFSS was determined using the microbond (or microdrop) micromechanical test, and the work of adhesion was estimated using two different procedures: (1) using the Owens and Wendt method, and (2) from the Dupre–Young expression using the contact angle θ of a cured epoxy resin on a single carbon fiber and the surface energy of the cured epoxy resin. It was found that the treatment of the carbon fiber with the silane-coupling agent appreciably increases its polar component because of the nitric acid oxidation and the chemisorption of the silane-coupling agent onto the carbon fiber surface. Also, the O=S=O group present in the polysulfone chain resin fairly increases the polar component of the epoxy–PSF blend. The results show that the wetting of the silane-treated carbon fiber by the thermoplastic-modified epoxy resin is better, thus increasing the fiber–matrix adhesion. It was also found that there is a similarity between the trends of both, the IFSS and the WA results. Also, from the ANOVA results it was also seen that both the incorporation of the PSF to the epoxy matrix and the surface treatment of the carbon fibers and their interaction were statistically significant to the IFSS and the WA.
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Cauich-Cupul Javier I.,Herrera-Franco Pedro J.,García-Hernández Edgar,Moreno-Chulim Veronica,Valadez-González Alex 한국탄소학회 2019 Carbon Letters Vol.29 No.4
A two-level full factorial design 22 with three replications was employed to assess the effect of the incorporation of PSF into the epoxy matrix and the surface treatment of carbon fibers on the work of adhesion (WA) and the interfacial shear strength (IFSS) of carbon fiber–epoxy composites. The IFSS was determined using the microbond (or microdrop) micromechanical test, and the work of adhesion was estimated using two different procedures: (1) using the Owens and Wendt method, and (2) from the Dupre–Young expression using the contact angle θ of a cured epoxy resin on a single carbon fiber and the surface energy of the cured epoxy resin. It was found that the treatment of the carbon fiber with the silane-coupling agent appreciably increases its polar component because of the nitric acid oxidation and the chemisorption of the silane-coupling agent onto the carbon fiber surface. Also, the O=S=O group present in the polysulfone chain resin fairly increases the polar component of the epoxy–PSF blend. The results show that the wetting of the silane-treated carbon fiber by the thermoplastic-modified epoxy resin is better, thus increasing the fiber–matrix adhesion. It was also found that there is a similarity between the trends of both, the IFSS and the WA results. Also, from the ANOVA results it was also seen that both the incorporation of the PSF to the epoxy matrix and the surface treatment of the carbon fibers and their interaction were statistically significant to the IFSS and the WA.
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H.J. Carrillo-Escalante,A. Álvarez-Castillo,A. Valadez-González,P. J. Herrera-Franco 한국탄소학회 2016 Carbon Letters Vol.19 No.-
In this study, the fracture behavior of a thermoplastic-modified epoxy resin reinforced with continuous carbon fibers for two levels of fiber-matrix adhesion was performed. A carbon fiber with commercial sizing was used and also treated with a known silane, (3-glycidoxy propyl trimethoxysilane) coupling agent. Toughness was determined using the double cantilever test, together with surface analysis after failure using scanning electron microscope. The presence of polysulfone particles improved the fracture behavior of the composite, but fiber-matrix adhesion seemed to play a very important role in the performance of the composite material. There appeared to be a synergy between the matrix modifier and the fibermatrix adhesion coupling agent.
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