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Microstructural evolution and strain-hardening behavior of multi-pass caliber-rolled Ti-13Nb-13Zr
Lee, T.,Park, K.T.,Lee, D.J.,Jeong, J.,Oh, S.H.,Kim, H.S.,Park, C.H.,Lee, C.S. Elsevier Sequoia 2015 Materials science & engineering. properties, micro Vol.648 No.-
The multi-pass caliber-rolling (MPCR) process is a rod-manufacturing process that has recently proven capable of fabricating ultrafine-grained bulk rods with superior mechanical performance for biomedical uses. There have rarely been studies which focused on MPCR-processed nonferrous alloys in spite of the great potential of doing so. The present work elucidates the metallurgical phenomena which occur during the MPCR process of Ti-13Nb-13Zr alloy, such as strain accumulation, microstructural evolution, and strain-hardening behavior. These factors were discussed in light of dislocation storage and annihilation. A FEM analysis revealed a significant amount of plastic strain applied by the MPCR process, most of which was considered as redundant strain. The heavy deformation induced a fragmentation of lamellar structure and strong grain refinement as the rolling passes increased in number. Both dynamic globularization and continuous dynamic recrystallization played key roles in such a microstructural change. In addition, a dislocation-based analysis provided further insight into the microstructural evolution and strain-hardening behavior of MPCR-processed titanium alloys.
Lee, T.,Lee, W.,Hyun, M.H.,Park, J.H. Elsevier 2010 Journal of chromatography Vol.1217 No.8
(-)-(18-Crown-6)-2,3,11,12-tetracarboxylic acid-bonded silica was used as the chiral stationary phase in capillary electrochromatography (CEC) for enantioseparation of some α-amino acids. Separation data in CEC were measured in mobile phases of varying pH, and composition of methanol and buffer, and compared with those in capillary liquid chromatography (CLC). In CEC better enantioseparation was generally obtained in the eluent of lower pH, higher buffer concentration and intermediate MeOH content, usually at the expense of analysis time. CEC showed generally better enantioselectivity and resolutions than CLC for the amino acids investigated.
Lee, T.,Chung, Y.H.,Yoon, J.,Min, J.,Choi, J.W. New York] ; North-Holland 2014 APPLIED SURFACE SCIENCE - Vol.320 No.-
In the present study, a fusion protein-based biofilm composed of a recombinant azurin-myoglobin (Azu-Myo) has been developed and confirmed its original electrochemical property for dual-level biomemory device application. For this purpose, the azurin was modified with cysteine residues for direct immobilization and conjugation. Then, the recombinant azurin was conjugated with the myoglobin via a sulfo-SMCC bifunctional linker using the chemical ligation method (CLM). The SDS-PAGE and UV-vis spectroscopy were performed to examine the fusion protein conjugates. The prepared Azu-Myo fusion protein was self-assembled onto Au substrate for the biofilm fabrication. Then, the atomic force microscopy (AFM) was used to confirm the immobilization and the surface-enhanced Raman spectroscopy (SERS) was carried out to the surface analysis. Also, the cyclic voltammetry (CV) was carried out to observe an electrochemical property of fabricated biofilm. As a result, the two pair of redox potential values was obtained for dual-level biomemory device application. Then, the dual-level biomemory function was verified by the multi-potential chronoamperometry (MPCA). The results indicate a new fabrication method and material combination for advances in bioelectronic device development.