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- 저자 : Bellum (검색결과 3 건)
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Infl uence of slag on mechanical and durability properties of fl y ash-based geopolymer concrete
Ramamohana Reddy Bellum,Karthikeyan Muniraj,Sri Rama Chand Madduru 한국세라믹학회 2020 한국세라믹학회지 Vol.57 No.5
A geopolymer binder is measured as an alternative and elective material to customary Portland binders. Utilization of Fly ash (FA) as a primary binding material limits the waste creation of thermal power stations and reduces environmental impacts. This paper presents the strength performance of geopolymer concrete (GC) with diff erent proportions of FA and ground granulated blast furnace slag. The potential of GC against acid resistance, porosity, water absorption, and sorptivity is presented in this paper. Apart from this, rapid chloride penetration test was performed to assess the chloride resistance of GC. XRD and SEM analysis was done on selected samples of GC to categorize microstructural performance. The results depicted that mixes M5 and M10 have attained higher compressive strengths, i.e., 49.0 and 57.6 MPa, while the acid durability loss factor values are less by 28% and 19%, respectively compared to other mixes of GC.
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Dasari Rekha,Jengiti. Dilip Kumar,Bellum Jayaraj,Y. Lingappa,Pattium Chiranjeevi* 대한화학회 2007 Bulletin of the Korean Chemical Society Vol.28 No.3
A micro organism Agrobacterium tumifacient as an immobilized cell on a solid support was presented as a new biosorbent in a simple and sensitive spectrophotometry determination of Ni(II) in various samples using 4-hydroxy benzaldehyde-4-bromophenyl hydrazone as a color developing agent (lmax 497 nm) at pH 4.0 0.2. Beers law was obeyed over the range of 0.01-0.1 g L-1. The molar absorptivity and Sandells sensitivity were 1.285 105 L mol-1cm-1 and 0.007245 g cm-2 respectively. Under these conditions, the preconcentration factor obtained was 82, and the detection limit achieved was 0.05 g L-1. The detailed study of various interfering ions made the method more sensitive and selective. The recovery of Ni(II) from various samples range from 97.75 to 99.35%. The present method was successfully applied for the determination of Ni(II) in spiked, natural water and alloy samples. The proposed method was compared with reported methods in terms of Students t-test and Variance ratio f-test which indicates that there is no significant difference between proposed and literature method at 95% confidence level.
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Rekha, Dasari,Kumar, Jengiti. Dilip,Jayaraj, Bellum,Lingappa, Y.,Chiranjeevi, Pattium Korean Chemical Society 2007 Bulletin of the Korean Chemical Society Vol.28 No.3
A micro organism Agrobacterium tumifacient as an immobilized cell on a solid support was presented as a new biosorbent in a simple and sensitive spectrophotometry determination of Ni(II) in various samples using 4-hydroxy benzaldehyde-4-bromophenyl hydrazone as a color developing agent (λmax 497 nm) at pH 4.0 ± 0.2. Beer's law was obeyed over the range of 0.01-0.1 μg L-1. The molar absorptivity and Sandell's sensitivity were 1.285 × 105 L mol-1cm-1 and 0.007245 μg cm-2 respectively. Under these conditions, the preconcentration factor obtained was 82, and the detection limit achieved was 0.05 μg L-1. The detailed study of various interfering ions made the method more sensitive and selective. The recovery of Ni(II) from various samples range from 97.75 to 99.35%. The present method was successfully applied for the determination of Ni(II) in spiked, natural water and alloy samples. The proposed method was compared with reported methods in terms of Student's ‘t'-test and Variance ratio ‘f'-test which indicates that there is no significant difference between proposed and literature method at 95% confidence level.
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