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Ziziphus spina-christi based bio-synthesis of Ag nanoparticles
Mervat F. Zayed,Wael H. Eisa,Yasser K. Abdel-Moneam,Salah M. El-kousy,Ahmed Atia 한국공업화학회 2015 Journal of Industrial and Engineering Chemistry Vol.23 No.-
The bio-production of silver nanoparticles (Ag NPs) using Ziziphus spina-christi extract was studied as a novel, rapid, low-cost and eco-friendly route. The impact of experimental factors, such as the extract quantity, precursor concentration and pH on the size and size distribution of Ag NPs, was studied with the aid of UV–vis spectrophotometer and transmission electron microscope (TEM). The FTIR analysis was carried out to identify the functional groups in Ag NPs. The as-synthesized Ag NPs was used as a catalyst for the reduction of 4-nitrophenol (4-NP) to 4-aminophenol (4-AP) in the presence of NaBH4.
Ahmed Atia,Yasser K. Abdel-Monem,A.H. Salama,Salah M. El-kousy,Wael H. Eisa 한국공업화학회 2023 Journal of Industrial and Engineering Chemistry Vol.117 No.-
A clean and high-throughput synthesis of gold@chitosan nanocomposite using nontoxic oxalic acid as areducing agent was developed. The synthetic route was carried out in completely dry conditions, i.e. solid-state reaction. The gold nanoparticles were bound with chitosan through the hydroxyl and aminogroups, as confirmed by Fourier transform infrared spectroscopic analysis. Scanning and transmissionelectron microscopy imaging confirmed the formation of semi-spherical gold particles with an averagesize of 8–15 nm. The catalytic performance of the synthesized gold nanoparticles for the reduction ofchromium(IV) in the presence of formic acid was evaluated. The film-forming ability of chitosan enabledthe design of separable/reusable heterogeneous catalyst which is convenient for real industrial applications. The proposed solid-state synthetic route could be adapted to produce a wide variety of nanostructuredmaterials that are characterized by high-yield, greenness, and low cost in very simple steps.