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A Review of Synthesis, Characterization and Applications of Copper Nanoparticles Using Green Method
Muhammad Rafique,Ahson J. Shaikh,Reena Rasheed,Muhammad Bilal Tahir,Hafiz FaiqBakhat,MUHAMMAD SHAHID RAFIQUE,Faiz Rabbani 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2017 NANO Vol.12 No.4
To address accosts of this modern age, the synthesis of metal nanoparticles is more important than ever. Copper has been recognized as a nontoxic, safe inorganic material, cheaper antibacterial/antifungal agent, and has high potential in a wide range of biological, catalytic and sensors applications more particularly in the form of nanoparticles. This resulted in the development of numerous methods for the synthesis of copper nanoparticles. As conventional methods like chemical and physical methods have several limitations so there is need to an alternate method. Due to nontoxic and eco-friendly nature, it has recently been shifted toward green synthesis of copper nanoparticles over conventional methods. Additionally, characterization of the synthesized nanoparticles is essential for their use in various applications. This review gives an overview of environment friendly synthesis method of copper nanoparticles and their applications on the basis of their potential selectivity and preferences in a number of fields like material sciences and biomedicine.
Rafique, Rafia,Zahra, Zahra,Virk, Nasar,Shahid, Muhammad,Pinelli, Eric,Park, Tae Jung,Kallerhoff, Jean,Arshad, Muhammad Elsevier 2018 Agriculture, ecosystems & environment Vol.255 No.-
<P>Titanium dioxide nanoparticles (TiO2 NPs) are used widely in commercial products. These high production levels have led to their increased release into natural ecosystems, where they may interact with plants and affect their physiological functions. The aim of this study was to assess the physiological responses of wheat (Triticum aestivum L.) to increasing concentrations of TiO2 NPs. TiO2 NPs with a particle size less than 20 nm were administered as soil spiked with 0, 20, 40, 60, 80, and 100 mg TiO2 NPs kg(-1), and their physiological parameters, including root and shoot lengths, biomass, phytoavailability of phosphorus (P), chlorophyll content, H2O2 production, and micronuclei (MN) formation in the plants grown from seeds in NPs-spiked soils, were subsequently recorded. All experiments were repeated twice with four replicates per treatment. After 60 days exposure to the NPs, root and shoot lengths, and P uptake by plants was significantly (p < 0.05) higher between 20 and 60 mg kg(-1) compared to the control (0 mg kg(-1) TiO2 NPs), but was then lower at 80 and 100 mg kg(-1) compared to 60 mg kg(-1) TiO2 NPs. The application of TiO2 NPs led to chlorophyll content being higher by 32.3% at 60 mg kg(-1) than in the control, but 11.1% lower content was observed at 100 mg kg(-1). The results suggested that wheat could not tolerate concentrations of TiO2 NPs higher than 60 mg kg(-1) owing to over-production of H2O2 (84.4%) and MN formation (53.6%).</P>
SELECTION OF A SUITABLE METHOD FOR THE SYNTHESIS OF COPPER NANOPARTICLES
ASIM UMER,SHAHID NAVEED,NAVEED RAMZAN,MUHAMMAD SHAHID RAFIQUE 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2012 NANO Vol.7 No.5
Various methods for the synthesis of copper nanoparticles employing chemical, physical and biological techniques considering bottom-up and top-down methods synthesis have been studied. The properties of copper nanoparticles depend largely on their synthesis procedures. The results from various investigations performed by di®erent scientists using these methods have been summarized. The applications, characterization techniques, advantages and disadvantages of each synthesis method are also the point of discussion. A detailed study of the results reveals that chemical reduction methods are most suitable for the synthesis of copper nanoparticles. Chemical reduction of copper salts using ascorbic acid (Vitamin C) is a new and green approach in which ascorbic acid is used both as the reduction and capping agent. This approach is the most e®ective and is also economical. Wide applications have been reported in various ¯elds, including heat transfer, catalyst production, electronics and medicine at a commercial scale. This process is nontoxic, environment-friendly and economical. The applications, characterization techniques, advantages and disadvantages of each synthesis method have been presented.