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Investigation of the Microstructure of Mechanically Milled Nd40Fe30Co15Al10B5 Alloy
Luu Tien Hung,Nguyen Huy Dan 한국물리학회 2008 THE JOURNAL OF THE KOREAN PHYSICAL SOCIETY Vol.52 No.5
The microstructure of Nd40Fe30Co15Al10B5 alloys fabricated by using a high-energy ball-milling method was investigated by using high-resolution transmission electron microscopy (HRTEM), scan- ning electron microscopy (SEM), energy dispersive X-ray analysis (EDX), selected area electron diraction (SAED) and electron backscatter diraction (EBSD) techniques. The crystalline phases found in the alloys were the tetragonal Nd2(Fe,Co,Al)14B (denoted as the 2 : 14 : 1 phase), the tetragonal Nd6(Fe,Co,Al)14 (denoted as the phase) and the fcc Nd-rich (a = 0.51 nm) phases. The formation of 2 : 14 : 1 crystallites supposedly contributed to the high coercivities up to 24 kOe for the alloys. The microstructure of Nd40Fe30Co15Al10B5 alloys fabricated by using a high-energy ball-milling method was investigated by using high-resolution transmission electron microscopy (HRTEM), scan- ning electron microscopy (SEM), energy dispersive X-ray analysis (EDX), selected area electron diraction (SAED) and electron backscatter diraction (EBSD) techniques. The crystalline phases found in the alloys were the tetragonal Nd2(Fe,Co,Al)14B (denoted as the 2 : 14 : 1 phase), the tetragonal Nd6(Fe,Co,Al)14 (denoted as the phase) and the fcc Nd-rich (a = 0.51 nm) phases. The formation of 2 : 14 : 1 crystallites supposedly contributed to the high coercivities up to 24 kOe for the alloys.
Structure and Magnetic Properties of Nd45-xCxFe30Co15Al10 Alloys
Nguyen Anh Tuan,Vu Hong Ky,Nguyen Huy Dan,Luu Tien Hung 한국물리학회 2008 THE JOURNAL OF THE KOREAN PHYSICAL SOCIETY Vol.52 No.5
Nd45-xCxFe30Co15Al10 (x = 0, 1, 3, 5 and 7) alloys were prepared by using a copper mold suction casting method. X-ray diraction (XRD) patterns show a trend of increasing crystallinity with increasing C content. In addition, crystallites with dierent shapes and sizes are observed by using scanning electron microscopy (SEM) and high-resolution transmission electron microscopy (HRTEM). Multi-phase properties of the alloys are clearly exhibited on the magnetic measurements. The hysteresis loops of the lower C content alloys (x = 1 and 3) show a single-phase hard magnetic behavior with coercivities of 6.2 kOe while the loops of the higher C content alloys (x = 5 and 7) are supposing a multi-phase property with coercivities up to 7.2 kOe. Two magnetic-phase transitions, depending on the C concentration, appear in the thermomagnetization curves. Addition of C at low content (1 to 3 at.%) can improve the hard magnetic behavior of the Nd-(Fe, Co)-Al alloy. Nd45-xCxFe30Co15Al10 (x = 0, 1, 3, 5 and 7) alloys were prepared by using a copper mold suction casting method. X-ray diraction (XRD) patterns show a trend of increasing crystallinity with increasing C content. In addition, crystallites with dierent shapes and sizes are observed by using scanning electron microscopy (SEM) and high-resolution transmission electron microscopy (HRTEM). Multi-phase properties of the alloys are clearly exhibited on the magnetic measurements. The hysteresis loops of the lower C content alloys (x = 1 and 3) show a single-phase hard magnetic behavior with coercivities of 6.2 kOe while the loops of the higher C content alloys (x = 5 and 7) are supposing a multi-phase property with coercivities up to 7.2 kOe. Two magnetic-phase transitions, depending on the C concentration, appear in the thermomagnetization curves. Addition of C at low content (1 to 3 at.%) can improve the hard magnetic behavior of the Nd-(Fe, Co)-Al alloy.
Tran Thi Minh Nguyet,Nguyen Cong Trang,Nguyen Quang Huan,Nguyen Xuan,Luu Tien Hung,Masakazu Date 한국물리학회 2008 THE JOURNAL OF THE KOREAN PHYSICAL SOCIETY Vol.52 No.5
Au=Fe₂O₃(Au : Fe = 1 : 50) catalyst was prepared by the co-precipitation method. The co- precipitate was studied by using dierential thermal analysis (DTA) and dierential thermal gravi- metric analysis (DTGA). The structure of the sample was investigated by using X-ray diraction (XRD) and transmission electron microscopy (TEM) and high-resolution transmission electron mi- croscopy (HRTEM). The particle size was determined to be within the range of 1.5 and 8 nm. Results of the study for catalytic properties showed that T1=2 for CO and H2 oxidation were 317 and 405 K respectively. Au=Fe₂O₃(Au : Fe = 1 : 50) catalyst was prepared by the co-precipitation method. The co-precipitate was studied by using DTA and DTGA. The structure of the sample was investigated by XRD, TEM and HRTEM. The particle size was determined to be within the range of 1.5 and 8 nm. Results of the study for catalytic properties showed that T1=2 for CO and H2 oxidation were 317 and 405 K respectively. Au=Fe₂O₃(Au : Fe = 1 : 50) catalyst was prepared by the co-precipitation method. The co- precipitate was studied by using dierential thermal analysis (DTA) and dierential thermal gravi- metric analysis (DTGA). The structure of the sample was investigated by using X-ray diraction (XRD) and transmission electron microscopy (TEM) and high-resolution transmission electron mi- croscopy (HRTEM). The particle size was determined to be within the range of 1.5 and 8 nm. Results of the study for catalytic properties showed that T1=2 for CO and H2 oxidation were 317 and 405 K respectively. Au=Fe₂O₃(Au : Fe = 1 : 50) catalyst was prepared by the co-precipitation method. The co-precipitate was studied by using DTA and DTGA. The structure of the sample was investigated by XRD, TEM and HRTEM. The particle size was determined to be within the range of 1.5 and 8 nm. Results of the study for catalytic properties showed that T1=2 for CO and H2 oxidation were 317 and 405 K respectively.
The Role of Zn Doping on the Catalytic Activity of the Nanoparticle Perovskite La0.7Sr0.3MnO3
Tran Thi Minh Nguyet,Nguyen Quang Huan,Tran Que Chi,Do The Chan,Nguyen Doan Thai,Nguyen Cong Trang,Luu Tien Hung,Le Van Tiep,Nguyen Van Qui 한국물리학회 2008 THE JOURNAL OF THE KOREAN PHYSICAL SOCIETY Vol.52 No.5
The nanometer complex oxide La0:7Sr0.3Mn0.6Zn0.₄O₃ was prepared by using a Sol-Gel method with citric acid as a ligand. The in uence of Zn doping of La0.7Sr0.₃MnO₃ on the structure, the morphology, the surface properties and on the catalytic activity of material was studied by using X-ray diraction (XRD), transmission electron microscopy (TEM), a high-resolution images and selected area electron diraction (SAED), physical adsorption and temperature programmed surface reaction (TPSR) methods. The results showed that perovskite La0:7Sr0:3Mn0:6. Zn0.₄O₃ could well catalyse propene oxidation in the temperature range 190 { 280 ℃, which was reduced to 100 { 120 ℃ for catalyst La1-χSrχMnO₃ The nanometer complex oxide La0:7Sr0.3Mn0.6Zn0.₄O₃ was prepared by using a Sol-Gel method with citric acid as a ligand. The in uence of Zn doping of La0.7Sr0.₃MnO₃ on the structure, the morphology, the surface properties and on the catalytic activity of material was studied by using X-ray diraction (XRD), transmission electron microscopy (TEM), a high-resolution images and selected area electron diraction (SAED), physical adsorption and temperature programmed surface reaction (TPSR) methods. The results showed that perovskite La0:7Sr0:3Mn0:6. Zn0.₄O₃ could well catalyse propene oxidation in the temperature range 190 { 280 ℃, which was reduced to 100 { 120 ℃ for catalyst La1-χSrχMnO₃