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- 검색키워드
- 저자 : F. H. Samuel (검색결과 2 건)
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Kh. A. Ragab,A. M. Samuel,A. M. A. Al-Ahmari,F. H. Samuel,H. W. Doty 대한금속·재료학회 2013 METALS AND MATERIALS International Vol.19 No.4
The current study investigates the influences of the fluidized bed heat treatment on the quality indices and microstructural characterization of A356.2 and B319.2 castings. Traditional heat treatment technology,employing circulating air convection furnaces (CF), was used to establish a relevant comparison with fluidized sand bed (FB) for the heat treatment of the alloys investigated, employing T6 continuous aging cycles or multi-temperature aging cycles. The results of alloys subjected to multi-temperature aging cycles reveal that the strength results obtained after the T6 continuous aging treatment of A356 alloys are not improved by means of multi-temperature aging cycles, indicating therefore that the optimum properties are obtained using a T6 aging treatment. The optimum strength properties of B319.2 alloys, however, is obtained by applying multi-temperature aging cycles such as, for example, 230 °C/2 h followed by 180 °C/8 h, rather than T6 aging treatment. In the case of multi-temperature aging cycles, the modification factor has the most significant role in improving the quality index values of 356 and 319 alloys. The FB heattreated alloys have the highest strength values for all heat treatment cycles compared to CF heat-treated alloys; however, the FB has no significant effect on the quality values of 319 alloys compared to the CF.
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Sohaimi Khairunissa Syairah Ahmad,Jaafar Juhana,Dharma Hadi Nugraha Cipta,Samuel Ojo,Ismail A. F.,Othman M. H. D.,Rahman Mukhlis A.,Aziz F.,Salleh W. N. W. 한국화학공학회 2024 Korean Journal of Chemical Engineering Vol.41 No.3
In this research, an innovative Z-scheme vanadium pentoxide (V 2 O 5 )/graphitic carbon nitride (g-C 3 N 4 ) photocatalyst was synthesised using a facile thermal treatment method, and its photodegradation performance and physicochemical properties were evaluated. The heterostructure provided high Brunauer–Emmett–Teller surface area and pore volume, which encouraged charge carrier separation and transfer, as well as supplied abundant micro-mesoporous structures and active sites for photocatalytic redox reactions. The successful incorporation of V 2 O 5 between g-C 3 N 4 layers can be proven by proposing the synthesis mechanism, as well as conducting morphology, crystal structure, elemental, and chemical analysis through scanning electron microscopy, X-ray diff raction, energy dispersive X-ray spectroscopy, and X-ray photoelectron spectroscopy, respectively. Using these combined photocatalysts, ciprofl oxacin (CIP) was successfully degraded up to 90.17% removal effi ciency in the visible-light spectrum. The superior photocatalytic activity of g-C 3 N 4 composite over V 2 O 5 is primarily due to its increased light absorption capacity, as well as increased surface area, pore size, and volume, eff ective charge transfer, and optimal band alignment between g-C 3 N 4 and V 2 O 5 . This research provides a signifi cant future perspective for the utilisation of Z-scheme V 2 O 5 /g-C 3 N 4 heterojunction photocatalyst for water treatment, especially those involving endocrine-disrupting compounds and antibiotics like CIP.
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