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Nadia Abdel Aal,M. Bououdina,A. Hajry,A. A. Chaudhry,J. A. Darr,A. A. Al-Ghamdi,E. H. El-Mossalamy,Attieh A. Al-Ghamdi,YongKielSung,Farid El-Tantawy 한국생체재료학회 2011 생체재료학회지 Vol.15 No.2
Hydroxyapatite(HAP) nanoparticles were successfully prepared from the biowaste chicken eggshells and phosphoric acid solution by chemical precipitation methods. The structures of HAP were characterized in terms of the X-ray diffraction (XRD), scanning electron microscope (SEM), and Fourier transform-infrared (FT-IR) spectroscopy. The effect of temperature on the crystallinity and lattice parameters of prepared HAP was monitored by X-ray powder diffraction. Energy dispersive X-ray analysis revealed that the HAP had a Ca/P molar ratio of about 1.65 and 1.69for as prepared and sintered HAP at 1200oC (1 hour), respectively. The temperature dependence on the electrical conductivity of sintered HAP nanoparticle was investigated. Furthermore, dielectric properties such as dielectric constant and dielectric loss as a function of frequency for the sintered HAP were also studied.
Carbon rich fly ash and their nanostructures
Numan Salah,Sami S. Habib,Zishan H. Khan,Ahmed Alshahrie,Adnan Memic,Attieh A. Al-ghamdi 한국탄소학회 2016 Carbon Letters Vol.19 No.-
Carbon rich fly ash was recently reported to have compositions that are ideal for use as a precursor and catalyst for carbon nanotube growth. This fly ash powder is mostly composed of pure carbon, predominantly present as sp2. In this work, the effect of sonication time on the morphology and structural properties of carbon rich fly ash particles is reported. The obtained results show that ultrasound treatment is an effective tool for producing ultrafine particles/fragments with higher porosity, which might be suitable for the adsorption of gasses. Moreover, carbon nanoparticles (CNPs) of this fly ash were produced in parallel using the ball milling technique, and were evaluated as reinforcements for epoxy based composites. These CNPs have almost spherical shapes with particle sizes of around 30 nm. They were found to have strong C=O carbonyl group bonds, which might be generated during the ball milling process. The tensile testing results of a fly ash CNP reinforced epoxy composite showed significant improvements in the mechanical properties, mainly in the stiffness of the polymer. The stiffness value was increased by around 23% of that of neat epoxy. These CNPs with chemically active groups might also be useful for other applications.