본 연구에서는 GC-FID를 이용하여 식품첨가물공전에 사용량이 정해져 있는 빵류, 캡슐류, 건조과실류·채소류 및 과실류·채소류 중 유동파라핀의 함량을 측정하였다. 시료에서 n-hexane으로 유...
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https://www.riss.kr/link?id=A99799557
2013
Korean
594
SCOPUS,KCI등재
학술저널
545-549(5쪽)
0
0
상세조회0
다운로드국문 초록 (Abstract)
본 연구에서는 GC-FID를 이용하여 식품첨가물공전에 사용량이 정해져 있는 빵류, 캡슐류, 건조과실류·채소류 및 과실류·채소류 중 유동파라핀의 함량을 측정하였다. 시료에서 n-hexane으로 유...
본 연구에서는 GC-FID를 이용하여 식품첨가물공전에 사용량이 정해져 있는 빵류, 캡슐류, 건조과실류·채소류 및 과실류·채소류 중 유동파라핀의 함량을 측정하였다. 시료에서 n-hexane으로 유동파라핀을 추출하고 KMnO4 산화반응을 통해 추출물 중불포화탄화수소의 극성을 증대시킨 다음 aluminium oxide를 충진한 SPE 카트리지로 정제하여 GC-FID로 측정하였다. 검출한계와 정량한계는 각각 10 ㎎/㎏과 20 ㎎/㎏으로 개별 n-alkane으로 정량하는 방법이 아닌 넓은 봉우리로 나타나는 유동파라핀의 면적의 합으로 정량하는 문헌들(15,17)의 값과 유사하게 나타났다. 유동파라핀은 빵류, 건조과실류·채소류 및 캡슐류에서 이형제 등으로 사용되고 있으나 최종 완제품에서 사용기준 이하로 검출되었고, 과실류·채소류에서 모두 불검출로 나타남에 따라 안전한 수준으로 관리되고 있음을 알 수 있었다.
다국어 초록 (Multilingual Abstract)
Liquid paraffin is a mixture of heavier alkanes derived from petroleum. It can be used as a lubricant in processing machinery, as a coating agent, or as a releasing agent. The purpose of this study was to analyze liquid paraffins in foods by using a g...
Liquid paraffin is a mixture of heavier alkanes derived from petroleum. It can be used as a lubricant in processing machinery, as a coating agent, or as a releasing agent. The purpose of this study was to analyze liquid paraffins in foods by using a gas chromatography-flame ionized detector (GC-FID). Liquid paraffin was extracted from the food samples using n-hexane. Non-polar aromatic or olefinic co-extractives were removed by alkaline permanganate oxidation followed by clean up on an aluminium oxide SPE cartridge before the GC-FID analysis. The results of recovery tests were 91.5-103.2%. Based on this optimized method, we investigated the amount of liquid paraffin in various food samples purchased from domestic markets. The levels of liquid paraffin in bread were 95.5±156.0 ㎎/㎏ (0.008%), those in capsules were 40.2±54.5 ㎎/㎏ (0.001%), and those in dried fruits and vegetables were 3.0±18.1 ㎎/㎏ (0.0001%). No liquid paraffin was detected in fresh fruits and vegetables. We propose that our method can be used to monitor and detect liquid paraffin in foods for food safety management.
참고문헌 (Reference)
1 Tennant DR, "The usage, occurrence and dietary intake of white mineral oils and waxes in Europe" 42 : 481-492, 2004
2 Bennet B, "Quantitative separation of aliphatic and aromatic hydrocarbons using silver ion-silica solid phase extraction" 72 : 1039-1044, 2000
3 Karasek L, "Proficiency test on the determination of mineral oil in sunflower oil. JRC Scientific and Technical Reports" European Communities 2009
4 Moret S, "Optimised off-line SPEGC- FID method for the determination of mineral oil saturated hydrocarbons (MOSH) in vegetable oils" 129 : 1898-1903, 2011
5 AOAC, "Official Methods of Analysis of AOAC International" Association of Official Analytical Communities 24-25, 2010
6 Moret S, "Mineral paraffins in olives and olive oils, In Olives and Olive Oil in Health and Disease Prevention" Elsevier 499-506, 2010
7 Vavasour E, "Mineral oils (medium- and low-viscosity) and paraffin waxes"
8 Food Standard Agency, "Mineral hydrocarbons in food contact materials"
9 KFDA, "Food Additives General and Safety Information" Korea Food and Drug Administration 1599-1603, 2005
10 Guinda, A, "Differences in hydrocarbons of virgin olive oils obtained from several olive varieties" 44 : 1723-1726, 1996
1 Tennant DR, "The usage, occurrence and dietary intake of white mineral oils and waxes in Europe" 42 : 481-492, 2004
2 Bennet B, "Quantitative separation of aliphatic and aromatic hydrocarbons using silver ion-silica solid phase extraction" 72 : 1039-1044, 2000
3 Karasek L, "Proficiency test on the determination of mineral oil in sunflower oil. JRC Scientific and Technical Reports" European Communities 2009
4 Moret S, "Optimised off-line SPEGC- FID method for the determination of mineral oil saturated hydrocarbons (MOSH) in vegetable oils" 129 : 1898-1903, 2011
5 AOAC, "Official Methods of Analysis of AOAC International" Association of Official Analytical Communities 24-25, 2010
6 Moret S, "Mineral paraffins in olives and olive oils, In Olives and Olive Oil in Health and Disease Prevention" Elsevier 499-506, 2010
7 Vavasour E, "Mineral oils (medium- and low-viscosity) and paraffin waxes"
8 Food Standard Agency, "Mineral hydrocarbons in food contact materials"
9 KFDA, "Food Additives General and Safety Information" Korea Food and Drug Administration 1599-1603, 2005
10 Guinda, A, "Differences in hydrocarbons of virgin olive oils obtained from several olive varieties" 44 : 1723-1726, 1996
11 Reich AG, "Dietary exposure assessment for direct and indirect food use applications for mineral hydrocarbones" 1998
12 Wagner C, "Determination of mineral paraffins on feeds and foodstuffs by bromination and preseparation on aluminium oxide: Method and results of a ring test" 92 : 231-249, 2001
13 Fiselier K, "Determination of mineral oil paraffins in foods by on-line HPLC-GC-FID: lowered detection limit; contamination of sunflower seeds and oils" 229 : 679-688, 2009
14 Koprivnjak O, "Determination of endogeneous aliphatic hydrocarbons of virgin olive oils of four autochthonous cultivars from Krk island (Croatia)" 35 : 125-131, 1997
15 Tanimura G, "Commentary of Analytical Metods for Food Additives in Food" Godansya 837-841, 1993
16 Fiselier K, "Activated aluminum oxide selectivity retaining long chain n-alkanes. Part I, description of the retention properties" 634 : 96-101, 2009
17 Fiorini D, "A versatile splitless injection GC-FID method for the determination of mineral oil paraffins in vegetable oils and dried fruit" 21 : 1155-1160, 2010
TMT 유도성 인지 기능 상실에 대한 대보(밤 품종) 내피 추출물의 효과
GC-MS를 이용한 바지락 중 prometryn 잔류분석법 확립
GC 및 GC/MS를 이용한 벌꿀 및 시판 음료 중의 Fructose, Glucose 및 Sucrose의 동시분석
열수추출조건이 동결건조 오미자의 추출 및 항산화 특성에 미치는 영향
학술지 이력
연월일 | 이력구분 | 이력상세 | 등재구분 |
---|---|---|---|
2023 | 평가예정 | 해외DB학술지평가 신청대상 (해외등재 학술지 평가) | |
2020-01-01 | 평가 | 등재학술지 유지 (해외등재 학술지 평가) | |
2010-11-23 | 학회명변경 | 영문명 : Korean Society Of Food Science And Biotechnology -> Korean Society of Food Science and Technology | |
2010-01-01 | 평가 | 등재학술지 유지 (등재유지) | |
2008-01-01 | 평가 | 등재학술지 유지 (등재유지) | |
2006-01-01 | 평가 | 등재학술지 유지 (등재유지) | |
2004-01-01 | 평가 | 등재학술지 유지 (등재유지) | |
2001-07-01 | 평가 | 등재학술지 선정 (등재후보2차) | |
1999-01-01 | 평가 | 등재후보학술지 선정 (신규평가) |
학술지 인용정보
기준연도 | WOS-KCI 통합IF(2년) | KCIF(2년) | KCIF(3년) |
---|---|---|---|
2016 | 1.03 | 1.03 | 1.1 |
KCIF(4년) | KCIF(5년) | 중심성지수(3년) | 즉시성지수 |
1.11 | 1.08 | 2.013 | 0.18 |