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      LC-MS/MS를 이용한 농산물 중 카벤다짐 분석 = Determination of Carbendazim in Commercial Agricultural Products by LC-MS/MS

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      https://www.riss.kr/link?id=A104515157

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      다국어 초록 (Multilingual Abstract) kakao i 다국어 번역

      A rapid and precise method using LC-MS/MS was developed for carbendazim analysis in agricultural products. This compound was extracted with acetonitrile from agricultural products and cleaned up by solidphase extraction procedure. The limit of detection and quantification were 0.001 mg/kg and 0.004 mg/kg, respectively.
      The mean recoveries and precision from 4 agricultural products, soybean sprout and mungbean sprout were in the range of 83.3-86.4% and 0.2-3.0% spiked at 1.0 mg/kg and those were in the range of 77.3-90.1% and 1.3-3.8% spiked at 0.02 mg/kg. The present method is faster and more precise compared with the multi-residue method of Korean Food Code. Therefore, we conclude that this method is suitable for carbendazim determination in a wide range of agricultural products.
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      A rapid and precise method using LC-MS/MS was developed for carbendazim analysis in agricultural products. This compound was extracted with acetonitrile from agricultural products and cleaned up by solidphase extraction procedure. The limit of detecti...

      A rapid and precise method using LC-MS/MS was developed for carbendazim analysis in agricultural products. This compound was extracted with acetonitrile from agricultural products and cleaned up by solidphase extraction procedure. The limit of detection and quantification were 0.001 mg/kg and 0.004 mg/kg, respectively.
      The mean recoveries and precision from 4 agricultural products, soybean sprout and mungbean sprout were in the range of 83.3-86.4% and 0.2-3.0% spiked at 1.0 mg/kg and those were in the range of 77.3-90.1% and 1.3-3.8% spiked at 0.02 mg/kg. The present method is faster and more precise compared with the multi-residue method of Korean Food Code. Therefore, we conclude that this method is suitable for carbendazim determination in a wide range of agricultural products.

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      참고문헌 (Reference)

      1 이제봉, "살균제 carbendazim이 랫드 간 해독체계에 미치는 영향" 한국농약과학회 9 (9): 338-346, 2005

      2 이제봉, "살균제 carbendazim이 DNA, 유전자 및 염색체에 미치는 영향" 한국농약과학회 8 (8): 288-298, 2004

      3 두옥주, "고상추출카트리지를 이용한 다중 잔류농약분석 시 정제용매에 따른 회수율 비교" 한국환경농학회 21 (21): 2-, 2002

      4 Bienvenida, G. L., "Study on the occurrence of pesticide residues in fruit-based soft drinks from the EU market and morocco using liquid chromatography-mass spectrometry" 26 : 341-346, 2012

      5 Chen, H., "Simultaneous determination of thiophanate-methyl and its metabolite carbendazim in tea using isotope dilution ultra performance liquid chromatography-tandem mass spectrometry" 165 : 1-8, 2013

      6 Razzino, C. A., "Sensitive determination of carbendazim in orange juice by electrode modified with hybrid material" 170 : 360-365, 2015

      7 Karunambigai, K., "Reverse phase high performance liquid chromatographic determination of residual carbendazim (fungicide) in raw and cooked indian cereals and pulses" 22 (22): 1-6, 2012

      8 Dioumaeva, I., "LC/MS/MS of Fungicides and Metabolites in Orange Juice with Agilent Bond Elut Plexa and Poroshell 120"

      9 김종율, "LC-MS/MS를 이용한 수도권에 유통되는 친환경 농산물의 잔류농약 모니터링 및 안전성 평가" 한국식품과학회 47 (47): 306-320, 2015

      10 Ministry of Food and Drug Safety, "Korea food code"

      1 이제봉, "살균제 carbendazim이 랫드 간 해독체계에 미치는 영향" 한국농약과학회 9 (9): 338-346, 2005

      2 이제봉, "살균제 carbendazim이 DNA, 유전자 및 염색체에 미치는 영향" 한국농약과학회 8 (8): 288-298, 2004

      3 두옥주, "고상추출카트리지를 이용한 다중 잔류농약분석 시 정제용매에 따른 회수율 비교" 한국환경농학회 21 (21): 2-, 2002

      4 Bienvenida, G. L., "Study on the occurrence of pesticide residues in fruit-based soft drinks from the EU market and morocco using liquid chromatography-mass spectrometry" 26 : 341-346, 2012

      5 Chen, H., "Simultaneous determination of thiophanate-methyl and its metabolite carbendazim in tea using isotope dilution ultra performance liquid chromatography-tandem mass spectrometry" 165 : 1-8, 2013

      6 Razzino, C. A., "Sensitive determination of carbendazim in orange juice by electrode modified with hybrid material" 170 : 360-365, 2015

      7 Karunambigai, K., "Reverse phase high performance liquid chromatographic determination of residual carbendazim (fungicide) in raw and cooked indian cereals and pulses" 22 (22): 1-6, 2012

      8 Dioumaeva, I., "LC/MS/MS of Fungicides and Metabolites in Orange Juice with Agilent Bond Elut Plexa and Poroshell 120"

      9 김종율, "LC-MS/MS를 이용한 수도권에 유통되는 친환경 농산물의 잔류농약 모니터링 및 안전성 평가" 한국식품과학회 47 (47): 306-320, 2015

      10 Ministry of Food and Drug Safety, "Korea food code"

      11 Lee, Y. D., "Handbook for the pesticide residue analytical methods of food code" National Institution of Food and Drug Safety Evaluation 78-82, 2012

      12 Hamdan, A.E., "Determination of some benzimidazole fungicides in tomato puree by high performance liquid chromatography with SampliQ polymer SCX solid phase extraction" 4 : 115-117, 2011

      13 Dujakovi, N., "Determination of pesticides in surface and ground waters by liquid chromatography-eletrospray-tandem mass spectrometry" 678 : 63-72, 2010

      14 Nakamura, M., "Determination of carbendazim, thiophanate, thiophanate-methyl and benomyl residues in agricultural products by liquid chromatography-tandem mass spectrometry" 52 (52): 148-155, 2011

      15 Hollosi, L., "Determination of carbendazim and benomyl residues in oranges and orange juice by automated online sample preparstion using TLX-LC-MS/MS"

      16 Kim, Y. G., "Determination and confirmation of the carbendazim residue in soybean sprout" 2 (2): 79-84, 1998

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      학술지 이력

      학술지 이력
      연월일 이력구분 이력상세 등재구분
      2026 평가예정 재인증평가 신청대상 (재인증)
      2020-01-01 평가 등재학술지 유지 (재인증) KCI등재
      2017-01-01 평가 등재학술지 유지 (계속평가) KCI등재
      2013-01-01 평가 등재학술지 유지 (등재유지) KCI등재
      2010-01-01 평가 등재학술지 선정 (등재후보2차) KCI등재
      2009-01-01 평가 등재후보 1차 PASS (등재후보1차) KCI등재후보
      2008-01-01 평가 등재후보 1차 FAIL (등재후보1차) KCI등재후보
      2006-07-21 학회명변경 영문명 : The Korean Sociery Of Food Hygiene And Safety -> The Korean Society of Food Hygiene and Safety KCI등재후보
      2006-01-01 평가 등재후보학술지 선정 (신규평가) KCI등재후보
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      학술지 인용정보

      학술지 인용정보
      기준연도 WOS-KCI 통합IF(2년) KCIF(2년) KCIF(3년)
      2016 0.45 0.45 0.48
      KCIF(4년) KCIF(5년) 중심성지수(3년) 즉시성지수
      0.49 0.49 0.726 0.08
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