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      Liquid type of fluorosulfonyl lithium salts containing siloxane for Li-ion electrolyte

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      https://www.riss.kr/link?id=A107484144

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      <P>Our goal in the present work is to synthesize liquid type of electrolyte that can be used in lithium-ion battery, based on fluorosulfonyl group. We synthesized a precursor of fluorosulfonyl isocyanate, and followed to prepare fluorosulfonyl carbamic acid ester lithium salt (SiFSC 1)s and fluorosulfonyl urea lithium salt (SiFSC 2)s containing siloxane electrolytes. Four electrolytes with carbamic or urea structures were prepared by changing the siloxane moieties with different chain length. The synthesized electrolytes are viscous liquid with different color. The resulting electrolytes were characterized by H-1 NMR spectroscopy and thermogravimetric analysis (TGA). The ionic conductivity of SiFSCs was compared by LiPF6 and LiFSI. (C) 2016 Published by Elsevier B.V. on behalf of The Korean Society of Industrial and Engineering Chemistry.</P>
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      <P>Our goal in the present work is to synthesize liquid type of electrolyte that can be used in lithium-ion battery, based on fluorosulfonyl group. We synthesized a precursor of fluorosulfonyl isocyanate, and followed to prepare fluorosulfonyl c...

      <P>Our goal in the present work is to synthesize liquid type of electrolyte that can be used in lithium-ion battery, based on fluorosulfonyl group. We synthesized a precursor of fluorosulfonyl isocyanate, and followed to prepare fluorosulfonyl carbamic acid ester lithium salt (SiFSC 1)s and fluorosulfonyl urea lithium salt (SiFSC 2)s containing siloxane electrolytes. Four electrolytes with carbamic or urea structures were prepared by changing the siloxane moieties with different chain length. The synthesized electrolytes are viscous liquid with different color. The resulting electrolytes were characterized by H-1 NMR spectroscopy and thermogravimetric analysis (TGA). The ionic conductivity of SiFSCs was compared by LiPF6 and LiFSI. (C) 2016 Published by Elsevier B.V. on behalf of The Korean Society of Industrial and Engineering Chemistry.</P>

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