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<P>4-Vinylbenzoyl azide was synthesized from p-vinylbenzoic acid and polymerized by free radical polymerization. The obtained polymer contained acyl azide groups which were thermally transformed to the corresponding isocyanato groups. Reactions ...
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RISS 인기검색어
https://www.riss.kr/link?id=A107571888
- 저자
- 발행기관
- 학술지명
- 권호사항
-
발행연도
2007
-
작성언어
-
- 주제어
-
등재정보
SCI,SCIE,SCOPUS
-
자료형태
학술저널
-
수록면
718-724(7쪽)
- 제공처
- 소장기관
-
0
상세조회 -
0
다운로드
부가정보
다국어 초록 (Multilingual Abstract)
<P>4-Vinylbenzoyl azide was synthesized from p-vinylbenzoic acid and polymerized by free radical polymerization. The obtained polymer contained acyl azide groups which were thermally transformed to the corresponding isocyanato groups. Reactions on these polymers with ethanol, hydroxyethyl methacrylate and 1-pyrenebutanol proceeded quantitatively. Time-resolved FT-IR studies of the reactions with ethanol were carried out by varying the concentration and temperature. The effect of the solvent polarity on the Curtius rearrangement was investigated.</P><P>
<img src='wiley_img/10221336-2007-28-6-MARC200600868-gra001.gif' alt='wiley_img/10221336-2007-28-6-MARC200600868-gra001'>
</P>
<img src='wiley_img/10221336-2007-28-6-MARC200600868-gra001.gif' alt='wiley_img/10221336-2007-28-6-MARC200600868-gra001'>
</P>
<P>4-Vinylbenzoyl azide was synthesized from p-vinylbenzoic acid and polymerized by free radical polymerization. The obtained polymer contained acyl azide groups which were thermally transformed to the corresponding isocyanato groups. Reactions on these polymers with ethanol, hydroxyethyl methacrylate and 1-pyrenebutanol proceeded quantitatively. Time-resolved FT-IR studies of the reactions with ethanol were carried out by varying the concentration and temperature. The effect of the solvent polarity on the Curtius rearrangement was investigated.</P><P>
<img src='wiley_img/10221336-2007-28-6-MARC200600868-gra001.gif' alt='wiley_img/10221336-2007-28-6-MARC200600868-gra001'>
</P>
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