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      2-Halobenzyl Phenyl Ether의 제조와 그 광화학 = The Synthesis and Photochemical Reaction of 2-Halobenzyl Phenyl Ether

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      https://www.riss.kr/link?id=A19666276

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      The photochemical reaction of 2-halobenzyl phenyl ethers was studied. In order to study the photoreactivity of haloarene tethered to arene with alkyl ether group, two 2-halobenzyl phenyl ethers were prepared. when the acetonitrile solution of 2-halobenzyl ethers in pyrex immersion vessel was irrdiated by 100W medium pressure Hg-lamp, the Photo-Fires type products, o(2-halo)benzyl phenol and p-(2-halo)benzyl phenol were obtained. Photo-Fires type reaction of 2-halobenzyl phenyl ether ws supposedly due to rearrangement of 2-halobenzyl radical and phenol radical produced by C_sp3-O bond cleavage. However when the reaction was carried out in benzene/aqueous alkalic solution with vycor immersion vessel, photocyclized product along the Photo-Fries type reaction products and photoreduced product was observed.
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      The photochemical reaction of 2-halobenzyl phenyl ethers was studied. In order to study the photoreactivity of haloarene tethered to arene with alkyl ether group, two 2-halobenzyl phenyl ethers were prepared. when the acetonitrile solution of 2-halobe...

      The photochemical reaction of 2-halobenzyl phenyl ethers was studied. In order to study the photoreactivity of haloarene tethered to arene with alkyl ether group, two 2-halobenzyl phenyl ethers were prepared. when the acetonitrile solution of 2-halobenzyl ethers in pyrex immersion vessel was irrdiated by 100W medium pressure Hg-lamp, the Photo-Fires type products, o(2-halo)benzyl phenol and p-(2-halo)benzyl phenol were obtained. Photo-Fires type reaction of 2-halobenzyl phenyl ether ws supposedly due to rearrangement of 2-halobenzyl radical and phenol radical produced by C_sp3-O bond cleavage. However when the reaction was carried out in benzene/aqueous alkalic solution with vycor immersion vessel, photocyclized product along the Photo-Fries type reaction products and photoreduced product was observed.

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