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      Synthesis and characterization of LiNiO_2 cathode material prepared by an adiphic acid-assisted sol-gel method for lithium secondary batteries

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      https://www.riss.kr/link?id=E689913

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      LiNiO_2(R3m) powders were synthesized by a sol-gel method using adiphic acid as a chelating agent. Highly crystallized LiNiO_2 was synthesized in oxygen at a calcination temperature of 750℃ for 14 h when molar ratio of adiphic acid to total metal ions was 1.0. The intensity ratio of (003)/(104) peaks of XRD spectrum for the synthesized material was 1.67. The LiNiO_2 powders were monodispersed particulate with the average size of approximately 1-2㎛. The electrochemical test of a half cell fabricated using the LiNiO_2 powders revealed that the cell had a high initial discharge capacity of 158 mAh g ^1 but it showed very fast capacity fading just after several tens of charge/discharge cycles. ⓒ 1999 Published by Elsevier Science B.V. All rights reserved.
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      LiNiO_2(R3m) powders were synthesized by a sol-gel method using adiphic acid as a chelating agent. Highly crystallized LiNiO_2 was synthesized in oxygen at a calcination temperature of 750℃ for 14 h when molar ratio of adiphic acid to total metal io...

      LiNiO_2(R3m) powders were synthesized by a sol-gel method using adiphic acid as a chelating agent. Highly crystallized LiNiO_2 was synthesized in oxygen at a calcination temperature of 750℃ for 14 h when molar ratio of adiphic acid to total metal ions was 1.0. The intensity ratio of (003)/(104) peaks of XRD spectrum for the synthesized material was 1.67. The LiNiO_2 powders were monodispersed particulate with the average size of approximately 1-2㎛. The electrochemical test of a half cell fabricated using the LiNiO_2 powders revealed that the cell had a high initial discharge capacity of 158 mAh g ^1 but it showed very fast capacity fading just after several tens of charge/discharge cycles. ⓒ 1999 Published by Elsevier Science B.V. All rights reserved.

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      목차 (Table of Contents)

      • Abstract
      • 1. Introduction
      • 2. Experimental
      • Abstract
      • 1. Introduction
      • 2. Experimental
      • 3. Results and discussion
      • 4. Conclusion
      • References
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