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あぁかがさざただなはばぱまやゃらわゎんいぃきぎしじちぢにひびぴみりうぅくぐすずつづっぬふぶぷむゆゅるえぇけげせぜてでねへべぺめれおぉこごそぞとどのほぼぽもよょろを

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고성능 액체 크로마토그래피에 의한 Costus speciosus중 Diosgenin의 분석법 = High-Performance Liquid Chromatographic Determination of the Diosgenin in Costus Speciosus

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https://www.riss.kr/link?id=A19619505

저자

朴奎昌 (慶熙大學校文理科大學化學科) ; 金宅濟 (韓國科學技術院化學分析室)
발행기관
慶熙大學校
학술지명
論文集
권호사항

Vol.14 No.- [1985]
발행연도
1985
작성언어
Korean
KDC
409.000
자료형태
학술저널
수록면

11-18(8쪽)
제공처
RISS
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다국어 초록 (Multilingual Abstract)

Diosgenin in Costus specious was analysed by high-performance liquid chromatographic (HPLC) Technique.
The dried, powdered sample was refluxed with the mixed solution of 3N HCl and xylene (1:1) at 95-100℃ for 4 hours.
The residue obtained from the xylene layer was acetylated and then injected into HPLC.
HPLC was performed using a set of four of the reversed-phase column (30㎝×3.9㎜ i.d., μ-Bondapak C_18, 10㎛) Connected in series.
The solvent system was tetrahydrofuran - n - hexane-acetonitrile (1:2:7). Au UV detector was used at a wavelenght of 210㎚.

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Diosgenin in Costus specious was analysed by high-performance liquid chromatographic (HPLC) Technique. The dried, powdered sample was refluxed with the mixed solution of 3N HCl and xylene (1:1) at 95-100℃ for 4 hours. The residue obtained from the...

Diosgenin in Costus specious was analysed by high-performance liquid chromatographic (HPLC) Technique.
The dried, powdered sample was refluxed with the mixed solution of 3N HCl and xylene (1:1) at 95-100℃ for 4 hours.
The residue obtained from the xylene layer was acetylated and then injected into HPLC.
HPLC was performed using a set of four of the reversed-phase column (30㎝×3.9㎜ i.d., μ-Bondapak C_18, 10㎛) Connected in series.
The solvent system was tetrahydrofuran - n - hexane-acetonitrile (1:2:7). Au UV detector was used at a wavelenght of 210㎚.