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This is to study the molar Ratio, the precipitation Condition and the Color of Nickel Sulfa-drugs Complexes. I Can observe the Colors of the Complexes Whenever precipitation Condition is obtained With PH 8~9 The molar ratio of Complexes is determined by gravimetric method and Solvent extraction method. By Both methods as above we found the molar ratio of Sulfadrugs and Nikel of indentified Complexes 2:1