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Stx119,pniowski, Wojciech J.,Choi, Jinsub,Yoo, Hyeonseok,Michalska-Domań,ska, Marta,Chilimoniuk, Paulina,Czujko, Tomasz North-Holland 2016 Materials letters Vol.164 No.-
<P><B>Abstract</B></P> <P>FeAl intermetallic alloy was anodized in 20wt% sulfuric acid at 0°C for 1min at the voltage ranging from 5 to 20V with a step of 2.5V. Based on the FE-SEM images, fast Fourier transformed (2D-FFT) quantitative arrangement analysis of the porous oxide was performed for the oxide formed after the first and the second step of anodization. It was found that for voltages below 15V FFT-derived regularity ratio values for both steps are comparable. For 15V and greater voltages regularity ratio of the obtained anodic oxide is much better while a two-step procedure is employed. Conducted research revealed that two-step self-organized anodization improves regularity of the porous oxide formed on FeAl intermetallic alloy. Moreover, regularity ratio increases rapidly with the anodizing voltage for the second step of anodization.</P> <P><B>Highlights</B></P> <P> <UL> <LI> FeAl intermetallic alloy was anodized in sulfuric acid. </LI> <LI> Porous oxide was obtained. </LI> <LI> Fast Fourier Transform based arrangement analysis was done. </LI> <LI> Since 15V, two-step anodizing improves arrangement. </LI> <LI> The greater voltage the better final arrangement of the pores. </LI> </UL> </P>