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이재욱,구정태,서정일,양창헌,이정호,이동철,이영현,이활,이경섭 동국대학교 경주대학 1997 東國論集 Vol.16 No.1
기종성 신우신염은 주로 당뇨병환자나 폐쇄성 요로질환을 가진 환자에 발생하며 특징적으로 신실질 및 그 주위조직에 가스를 형성하면서 심한 조직괴사를 일으키는 매우 드문 급성 화농성 신감염으로 사망률이 높은 질환이다. 이 질환은 1989년 Kelly와 MacCallum에 의해 처음 보고된 이래 외국문헌에 약 90례 정도가 보고되어 있으며 국내에는 28례가 보고되어 있다. 수액 및 전해질 보충, 인슐린 투여를 통한 적절한 혈당조절 및 항생제 투여등의 내과적 치료와 절개배농 및 신적출술등의 수술적 치료 방법이 있다. 내과적 치료로 가스의 감소가 없는 경우에는 즉각적인 수술적 치료를 시행하여야하므로 이 가스변화에 대한 추적관찰이 중요하다 하겠다. 본 저자들은 당뇨병환자에서 발생한 기종성 신우신염 1례를 내과적 요법을 치험하였기에 문헌고찰과 함께 보고하고자 한다. Emphysematous pyelonephritis is rare, life-threatening infection of the renal parenchyma and perirenal tisseue. This disease is characterized by the production of intrarenal and perirenal gas and is frequently encountered in patients with diabetes mellitus or urinary obstruction. We experienced a case of emphysematouse pyelonephritis in a 62 years old women with poorly controlled diabetes mellitus who had been managed with medical theraphy. So we report this case with a review of the referenced literatures.
Zeolite X 촉매를 이용한 WO₃의 CO 환원-탄화반응
이동활,이종대,전진혁,박노국,류시옥,이태진 嶺南大學校 工業技術硏究所 2003 工業技術硏究所論文集 Vol.31 No.2
This study was performed to manufacture tungsten carbide from CO reduction- carburization of WO₃using zeolite-NaX catalyst. Zeolite-NaX catalyst could improve the reduction property of WO₃. Moreover, zeoite-HX and KX catalysts also improved the reduction property of WO₃. This improvement of reduction property leaded to the decrease of reaction temperature. The size of WC particle was 50∼60 nm at 650 ℃ for 10h. From these results, it is concluded that the various zeolite X catalysts could be used for the reduction-carburization of W0₃ as the catalysts.
WO_3의 환원-탄화에 있어서 Zeolite NaX, HX, KX의 특성에 따른 영향
이동활,이종대,박영효,박노국,이태진 한국공업화학회 2003 응용화학 Vol.7 No.1
The effect of the Zeolite HX,NaX, and KH prepared by ion-exchange method, on the reduction-carburization of WO_3 was studied This study was performed at thetemperature range from 300℃ to 735 ℃ with CO gas. The produced gas, CO_2, was analyzed by mass spectroscopt The addition of the Zeolite HX, NaX,and KX into WO_3 increased the efficiency of the reduction-carburization of WO_3 and Zeolite HX with the strongest acidity was the most effective on redution-carburization among them. The Zeolite HX, NaX, and KX improved the oxygen mobility of WO_3 and the acidity of the Zeolite was directly related to the increasing efficiency of reduction-carbuization of WO_3.
The preparation of nanophase tungsten carbide powder with zeolite-X catalysts
Lee, Jong Dae,Lee, Dong-Hwal,Park, No-Kuk,Ryu, Si Ok,Lee, Tae Jin Elsevier 2006 CURRENT APPLIED PHYSICS Vol.6 No.6
<P><B>Abstract</B></P><P>The reduction–carburization of tungsten trioxide (WO<SUB>3</SUB>) under carbon monoxide flow was studied in the temperature range of 300–750°C. The reduction–carburization of WO<SUB>3</SUB> was improved by mechanically mixing with zeolite-HX, -NaX and -KX. The interaction between cation in zeolite-X and oxygen in WO<SUB>3</SUB> affected the improvement of the reduction–carburization of WO<SUB>3</SUB> to WC. Moreover, the improved reduction–carburization of WO<SUB>3</SUB> could lead to the decrease of reaction temperature. Because the particle size of WC is in contact with a reaction temperature, the nanophase WC can be prepared at low temperature. In particular, the particle size of WC was controlled by reaction temperature. The particle sizes of produced WC at 550, 650 and 700°C were 25, 50 and 100nm respectively.</P>