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MMA 이중 플랜지를 갖는 GFRP 복합관 구조거동에 관한 실험 연구 (II)
Ji, Hyo-Seon,El-Badry Mamdouh 한국복합신소재구조학회 2015 복합신소재구조학회논문집 Vol.6 No.3
This paper presents on the structural behavior of the the methyl methacrylate monomer (MMA) double wide flanged the glass fiber-reinforced polymer(GFRP) pipe composite structures for the manhole raise. The evaluation of structural performance on this composite structure was conducted by the axial load, fatigue load, and ultimate load test. The assessment indicates that the MMA double wide flanged GFRP pipe composite structures was confirmed safety, durability and reliability in result as expected. It was found that this composite structure was able to short working times to around 30-50% and construction costs to around 10-23% with compare other construction methods. Also, environmental pollution and civil complaints will be prevented because there will be no longer any noises, vibrations, dust, or construction wastes.
Ji, Hyo-Seon,El-Badry Mamdouh 한국복합신소재구조학회 2015 복합신소재구조학회논문집 Vol.6 No.3
The repair of manhole raise has been caused much construction times and disruption of traffic flow, serious environmental pollution from crushed construction wastes, and budget waste due to the repeated repair construction works. In order to overcome such problems, we have developed the new manhole repairing composite structures by using a glass fiber-reinforced polymer (GFRP) pipe, which can raise manhole to the regular height of the overlayed road pavement with rapid construction and minimum traffic jams. This environmental-friendly technology is method completed by the methyl methacrylate monomer (MMA) double wide flanged GFRP pipe composite structures in order to raise manhole to the regular height. In this paper, two kinds of the compressive strength tests of MMA mortar composites were conducted and evaluated by a general compressive strength test, and compressive strength test after freezing-thawing resistance test. It was found that this MMA mortar composites will be used for the application of the double wide flanged GFRP pipe composite structures.
El-Badry, Susan M.,Taha, Mamdouh A.M. Korean Chemical Society 2014 대한화학회지 Vol.58 No.4
A series of new $N^7$-tetrazolo[5,1-f ]-1,2,4-triazin-8-(7H)-one derivatives 4-16 were designed and synthesized from 3 with different reagents. The newly prepared compounds were characterized by spectral data and screened for their antimicrobial activities against various bacteria and fungi strains.
El-Badry, Susan M.,Taha, Mamdouh A.M. Korean Chemical Society 2011 대한화학회지 Vol.55 No.6
Ethyl 1-aminotetrazole-5-carboxylate (1) has been utilized to construct a variety of novel tetrazolo [1,5-b]-1,2,5-oxadiazepine derivatives which repesent a relatively little explored group with interesting antibacterial activities. The synthesized compounds were elucidated using IR, $^1H$ NMR and mass spectroscopic methods, besides elemental analyses.
Taha, Mamdouh A. M.,El-Badry, Susan M. Korean Chemical Society 2010 대한화학회지 Vol.54 No.4
Ethyl 1-aminotetrazole-5-carboxylate (1)를 hydrazine hydrate와 반응시켜서 대응하는aminohydrazide 2를 합성한 후에, 화합물 2를carbon disulfide와 반응시켜서 1,3,4-oxadiazole-5-thiol structure 3을 합성하였다. 얻어진 화합물 3을 either chloroacetone 또는 ethyl chloroacetate와 반응시켜서S-acyl 1,3,4-oxadiazole 유도체인 4 와 5를 합성하였으며, 또한 hydrazine hydrate와 반응시켜서 4-amino-1,2,4-triazole-5-thiol 유도체인 6을 합성하였으며, 화합물 6을 glacial acetic acid와 반응시켜서 6-methyl-1,3,4-triazolo[3,4-b]-1,3,4-thiadiazole (7)을 합성하였다. 한편, 알려진 방법에 따라서, 화합물 1로부터 tetrazolo[5,1-f]-1,2,4-triazine 9을 얻은 다음에, 화합물 9를 carbon disulfide와 반응시켜서 8-thione 유도체인 10을 합성한 후에, 대응하는 화합물 11, 12 및 13을 합성하였다. 얻어진 화합물13을 이용하여1,2,4-triazolo[4,3-d]tetrazolo[5,1-f]-1,2,4-triazines 14와 15를 합성하였다. 새롭게 합성한 화합물들의 화학구조를 확인하였으며, 합성한 화합물들에 대한 항균 활성시험을 수행하였다. Ethyl 1-aminotetrazole-5-carboxylate (1) reacted with hydrazine hydrate to give the corresponding aminohydrazide 2. Cyclization of 2 by carbon disulfide yielded 1,3,4-oxadiazole-5-thiol structure 3. Reaction of 3 with either chloroacetone or ethyl chloroacetate furnished S-acyl 1,3,4-oxadiazole derivatives 4 and 5, respectively. Also compound 3 reacted with hydrazine hydrate afforded 4-amino-1,2,4-triazole-5-thiol derivative 6. 6-Methyl-1,3,4-triazolo[3,4-b]-1,3,4-thiadiazole structure 7 was synthesized by reaction of aminothiol 6 with glacial acetic acid. Diazotization of 1 with sodium nitrite in presence of hydrochloric acid yielding the diazonium salt which on treating with hippuric acid, oxazolone derivative 8 was obtained. Furthermore, tetrazolo[5,1-f]-1,2,4-triazine 9 was constructed via cyclization of aminoester 1 with formamide. Compound 9 reacted with carbon disulfide to furnish 8-thione derivative 10 which reacting with chloroacetone, ethyl chloroacetate, and hydrazine hydrate, the corresponding chemical structures 11, 12, and 13 were synthesized. 1,2,4-Triazolo[4,3-d]tetrazolo[5,1-f]-1,2,4-triazines 14 and 15 were resulted by treating of compound 13 with triethyl orthoformate, and glacial acetic acid, respectively. The structures of the newly synthesized products were elucidated according to elemental analyses and spectroscopic evidences. Some of the representative members of the prepared compounds were screened for antimicrobial activity.
지효선 ( Hyo Seon Ji ),( El Badry Mamdouh ) 한국복합신소재구조학회 2015 복합신소재학회논문집 Vol.6 No.3
The repair of manhole raise has been caused much construction times and disruption of traffic flow, serious environmental pollution from crushed construction wastes, and budget waste due to the repeated repair construction works. In order to overcome such problems, we have developed the new manhole repairing composite structures by using a glass fiber-reinforced polymer (GFRP) pipe, which can raise manhole to the regular height of the overlayed road pavement with rapid construction and minimum traffic jams. This environmental-friendly technology is method completed by the methyl methacrylate monomer (MMA) double wide flanged GFRP pipe composite structures in order to raise manhole to the regular height. In this paper, two kinds of the compressive strength tests of MMA mortar composites were conducted and evaluated by a general compressive strength test, and compressive strength test after freezing-thawing resistance test. It was found that this MMA mortar composites will be used for the application of the double wide flanged GFRP pipe composite structures.
MMA 이중 플랜지를 갖는 GFRP 복합관 구조거동에 관한 실험 연구(2)
지효선 ( Hyo Seon Ji ),( El Badry Mamdouh ) 한국복합신소재구조학회 2015 복합신소재학회논문집 Vol.6 No.3
This paper presents on the structural behavior of the the methyl methacrylate monomer (MMA) double wide flanged the glass fiber-reinforced polymer(GFRP) pipe composite structures for the manhole raise. The evaluation of structural performance on this composite structure was conducted by the axial load, fatigue load, and ultimate load test. The assessment indicates that the MMA double wide flanged GFRP pipe composite structures was confirmed safety, durability and reliability in result as expected. It was found that this composite structure was able to short working times to around 30-50% and construction costs to around 10-23% with compare other construction methods. Also, environmental pollution and civil complaints will be prevented because there will be no longer any noises, vibrations, dust, or construction wastes.