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임응극,정수진,김석영 한국세라믹학회 1982 한국세라믹학회지 Vol.19 No.4
A new perovskite type compound, (Pb1a-χKy□χ-y) (Zr0.33Ti0.67)O3-χ+y/2 was proposed and synthesized by "Wet-Dry Combination Technique". This defect ferroelectric material was characterized by partial substitutions of K+ for Pb+2 in Pb(Zr0.33Ti0.67)O3. This material was mono-phasic perovskite compound at 800℃ for 1hr., but ZrO2 was more or less isolated from the (Pb1a-χKy□χ-y) (Zr0.33Ti0.67)O3-χ+y/2. As a result, snitering temperature, sintered density, curie temperature, and dielectric constant of test pieces decreased and a-axis was nearly constant, while c-axis gradually decreased with the value x in the region of tetragonal phase of PZT. It was also recognized that the defect structure caused by adding K+ was found in both A-site cation and O-site anion vacancies in the defect PZT.
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임응극,정수진,유강수 한국세라믹학회 1983 한국세라믹학회지 Vol.20 No.3
The dielectric and piezoelectic properties in which $(Zr_{0.52} Ti_{0.48})^{+4}$ ions of $Pb(Zr_{0.52} Ti_{0.48})O_3$ are partially substituted for $W^{+6}$ ions were studied. $ZrTiO_4$ was made by coprecipitation. The specimens of disc shape were sintered respectively at 1180$^{\circ}$to 130$0^{\circ}C$ at an intervals of 2$0^{\circ}C$ for 1 hour. The optimum sintering temperature were found to be between 126$0^{\circ}C$ and 128$0^{\circ}C$. PZT solid solutions sintered had the tetragonal structure with c/a=1.025$\pm$0.005 and theoretical densities incre-ased from 8.02 to 8.17g/cm3 with increasing the amount of the partial substitution of $(Zr_{0.52} Ti_{0.48})^{+4}$ ion for $W^{+6}$ ion The grain size and curie temperature decreased with increasing the amount of $WO_3$ while the dielectric constant increased. When $(Zr_{0.52} Ti_{0.48})^{+4}$ ion was substituted for 1 mole% of $W{+6 ]$ion the planar coupling coefficient$(K_P)$ was as high as 0.58 But as the amount of $WO_3$ increased the mechanical quality factor(Qm) decreased considerably.
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임응극,Lim Eung Keuk 한국시멘트협회 1973 시멘트 심포지움 Vol. No.
A historical review of burning processes on cement manufacture has been made regarding specially to heat efficiency. In addition to these processes, two examples of stoichiometric calculation dealing with combustion such as air fuel ratio and excess air h
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Effect of Composition Variation and Particle Size of a Bristol Glaze
임응극,Eung Keuk Lim Korean Chemical Society 1963 대한화학회지 Vol.7 No.2
브리스톨釉藥을 콘 5, 8, 11 番으로 燒成했을때 나타나는 狀態에 對한 組成變化와 粒度의 京鄕을 硏究하여, 밝은 半艶消 또는 艶消釉藥을 얻을 수 있었다. 卽 各 釉藥에 對한 熱成範圍, 曲强度 및 光澤, 平滑性, 乳白度, Eggshelling, 龜裂, Pinholing, Crawling 等에 對한 因子를 決定하므로서 얼마나, 珪酸, 알카리, 石灰를 變化시켜 實際 使用可能한 良好한 釉藥을 얻었다. 製造된 브리스톨釉藥은 最低 콘 5番부터 11번 또는 그 以上에서 긴 熟成範圍를 나타냈다. Crawling의 傾向에 있어서는 ZnO 量이 增加될때 特히 甚했으나, $Al_2O_4:\;SiO_2$의 比가 크고 ZnO 量이 많을때 乳白度가 顯著하였다. 釉藥의 粒子를 가늘게 하면 熱成이 잘되나 微粒이면 Crawling이 커진다. 釉藥두께를 增加해도 Crawling 傾向이 커진다. A study was made of the effect of composition changes and particle size on appearance of raw bristol glazes fired at cones 5, 8, and 11. Alumina and silica, alkali and lime variations were made to get some of the more promising glazes determining maturing ranges, modulus of rupture, and other factors such as gloss, smoothness, opacity, eggshelling, crazing, pinholing and crawling for each glaze. Modulus of rupture was measured for the glazes fired at only cone 11.
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임응극,박순자,정수진,김환,Lim, Eung-Keuk,Park, Soon-Ja,Chung, Su-Jin,Kim, Hwan 한국세라믹학회 1980 한국세라믹학회지 Vol.17 No.1
Mineral identifications on halloysite in Hadong-Sancheong area and the halloysite bearing clay ii Yeoju, Yesan and Hampyeong-Muan area are carried out by the method of X-ray diffraction, electron microscopy and DTA. Chemical composition of the above minerals are analyzed by means of X-ray-fluorescence. Refractoriness are also measured by refractoriness tester. A standard diagram for quantitative analysis of halloysite is given.
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Dielectric Behavior of Steatite Body
임응극,Eung Keuk Lim Korean Chemical Society 1963 대한화학회지 Vol.7 No.2
粘土鑛物과 滑石과의 關係에 對한 正確한 報告가 거의 없어. 이에 對한 磁器化溫度範圍 및 電氣的絶緣性과 粘土含量의 關係를 究明하였다. 스테아타이트素地의 製造에 使用한 原料는 國産 滑石, 粘土, 長石, 硅石等이며, 吸水率, 燒成線收縮率을 測定 檢討하고, 또 磁器化된 素地들의 電氣的絶緣性을 測定하였다. 그 結果 磁器化溫度範圍는 재겔錐 1乃至 3番內에 있었으며 $MgCO_3$를 添加함에 따라 燒成收縮은 크게 일어났으나, 粘土含量이 20% 以下였을 때는 磁器化溫度範圍가 增大되었다. 耐熱性은 全般的으로 良好하였으며 粘土量을 增加시킴에 따라 膨脹率, 誘電體力率, 絶線耐性은 增加하고, 體積固有抵抗은 減少하였다. A review of the literature is cited. Little exact information exists on the relation between clay materials and talc. The raw materials which are used in making steatite body consist of talc, clay, feldspar, and flint mined in Korea. The percentage absorption and linear burning shrinkage are measured and then discussed. The vitrified bodies were used in measurement of dielectric properties. The method of measurements for dielectric properties are described too.
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