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Interfacial Characteristics of Epoxy Composites Filled with γ-APS Treated Natural Zeolite
이재영,이상근,김상욱,Lee, Jae-Young,Lee, Sang-Keun,Kim, Sang-Wook 한국접착및계면학회 2001 접착 및 계면 Vol.2 No.3
${\gamma}$-APS (${\gamma}$-aminopropyltriethoxysilane)로 표면처리된 천연제올라이트와 에폭시 수지 복합 재료의 표면 자유 에너지, 인상강도 및 계면 모폴로지에 대해 연구하였다. 표면처리하지 천연제올라이트의 표면 자유에너지 성분 중에서 무극성 성분인 Lifshitz-van der Waals 성분, ${\gamma}{\frac{LW}{SV}}$는 $19.22mJ/m^2$이었고, 극성 성분인 Lewis acid-base 성분, ${\gamma}{\frac{AB}{SV}}$는 $15.27mJ/m^2$이 있다. ${\gamma}$-APS의 처리농도가 증가함에 따라 ${\gamma}{\frac{LW}{SV}}$값은 증가하였지만 ${\gamma}{\frac{AB}{SV}}$는 감소하였으며, 이는 ${\gamma}$-APS의 소수성 성분인 알킬기의 영향이 친수성 기인 아민이나 수산기의 영향보다 커지기 때문이다. 인장강도와 Young율은 ${\gamma}$-APS 처리에 의해 개선되었으며, SEM 분석에 의해 계면특성이 향상되었음을 확인하였다. Epoxy composites filled with natural zeolite was prepared to investigate the effects of silane coupling agent, ${\gamma}$-APS (${\gamma}$-aminopropyltriethoxysilane)on the surface free energy, tensile properties and interfacial morphology. The value of Lifshitz-van der Waals component, ${\gamma}{\frac{LW}{SV}}$ for polar was $19.22mJ/m^2$ and increased, while that of Lewis acid-base component, ${\gamma}{\frac{AB}{SV}}$ for polar was $15.27mJ/m^2$ and decreased with the increasing content of ${\gamma}$-APS treatment. It is due that the surface of the zeolite is more coated by hydrophobic of alkyl group than hydrophilic amine or hydroxyl group. The tensile strength and Young's modulus of epoxy system were improved by the treatment with ${\gamma}$-APS due to the strong interface bonding, which was confirmed by SEM.
PET/CT 감쇠보정시 다양한 CT Kernel 적용에 따른 유용성 평가
이재영,성용준,윤석환,박찬록,이홍재,노경운,Lee, Jae-Young,Seong, Yong-Jun,Yoon, Seok-Hwan,Park, Chan-Rok,Lee, Hong-Jae,Noh, Kyung-Wun 대한핵의학기술학회 2017 핵의학 기술 Vol.21 No.2
PET/CT 영상 재구성시 감쇠보정맵을 사용하여 영상재구성에 적용한다. 감쇠보정 맵의 CT parameter을 변경하여 PET/CT 영상 재구성 할 때 적용하여 SUVmax에 어떤 영향을 미치는지 비교 평가해보고자 한다. 장비는 Biograph mCT 64를 사용하였고 Phantom은 NEMA IEC Body Phantom을 사용하였다. 실험을 위해 환자는 2017년 2월에서 3월까지 본원 PET/CT 검사를 시행한 환자 20명을 대상으로 Lung, Liver, Bone에 관심영역을 선택하여 기존 08f AC, 45f medium, 80f ultra sharp 방식의 CT kernel을 적용한 감쇠보정맵을 사용하여 PET/CT 영상 재구성에 도입 후 방사능 농도(kBq/mL), SUVmax, SD(standard deviation) 변화 유무를 평가하였다. Phantom 방사능 농도 측정 결과 B08f AC 대비 B45f 0.96%, B80f 6.58% 증가하였고 B08f AC 대비 B45f 0.86%, B80f 6.54%각각 증가하였고, SD의 경우 B08f AC 대비 B45f 1.27%, B80f 6.96% 증가하였다. 환자에서 부위별 SUV는 Lung에서 B08f AC 대비 B45f 1.6%, B80f 6.6%, Liver에서 B08f AC 대비 B45f 0.7%, B80f 4.7%, Bone에서 B08f AC 대비 B45f 1.3%, B80f 6.2% 증가를 보였다. 부위별 SD는 Lung에서 B08f AC 대비 B45f 6.2%, B80f 15.4%, Liver에서 B08f AC 대비 B45f 2.1%, B80f 11%, Bone에서 B08f AC 대비 B45f 를 사용할 때 2.3%, B80f 14.7% 증가를 보였다. CT Kernel변화에 따라 sharpness noise와 영상의 질은 변화를 보였으나 SUVmax와 SD는 통계적으로 유의한 차이가 없었다.(P>.05). 핵의학 영상은 정량적인 평가가 중요하다 따라서 부위에 따라 CT kernel이 적절하게 조절되고 noise level이 낮은 감쇠보정 맵을 사용하여 PET/CT 재구성시에 적용하여 정량적 평가에 오류를 줄이는 것이 중요하다고 사료되므로 따라서 같은 부위라 할지라도 sharpness noise가 인위적으로 증가된 kernel을 사용하는 것보다 noise가 낮은 kernel을 사용하는 것이 SD편차를 줄이고 정량적인 평가에 오류를 적게 하여 정확한 진단과 SUV 측정에 유용할 것으로 사료된다. Purpose Recently PET/CT image's attenuation correction is used CTAC(Computed Tomgraphy Attenuation Correction). it can quantitative evaluation by SUV(Standard Uptake Value). This study's purpose is to evaluate SUV and to find proper CT kernel using CTAC with applied various CT kernel to PET/CT construction. Materials and Methods Biograph mCT 64 was used for the equipment. We were performed on 20 patients who had examed at our hospital from february through March 2017. Using NEMA IEC Body Phantom, The data was reconstructed PET/CT images with CTAC appiled various CT kernel. ANOVA was used to evaluated the significant difference in the result. Results The result of measuring the radioactivity concentration of Phantom was B45F 96% and B80F 6.58% against B08F CT kernel, each respectively. the SUVmax increased to B45F 0.86% and B80F 6.54% against B08F CT kernel, In case of patient's parts data, the Lung SUVmax increased to B45F 1.6% and B80F 6.6%, Liver SUVmax increased to B45F 0.7% and B80F 4.7%, and Bone SUVmax increased to B45F 1.3% and B80F 6.2%, respectively. As for parts of patient's about Standard Deviation(SD), the Lung SD increased to B45F 4.2% and B80F 15.4%, Liver SD increased to B45F 2.1% and B80F 11%, and Bone SD increased to B45F 2.3% and B80F 14.7%, respectively. There was no significant difference discovered in three CT kernel (P >.05). Conclusion When using increased noise CT kernel for PET/CT reconstruction, It tends to change both SUVmax and SD in ROI(region of interest), Due to the increase the CT kernel number, Sharp noise increased in ROI. so SUVmax and SD were highly measured, but there was no statistically significant difference. Therefore Using CT kernel of low variation of SD occur less variation of SUV.
레이저 키홀 용접의 열원 모델링: Part 2-간극과 두께 차이의 영향
이재영,이원범,유중돈,Lee Jae-Young,Lee Won-Beom,Yoo Choong-Don 대한용접접합학회 2005 대한용접·접합학회지 Vol.23 No.1
A three-dimensional Gaussian heat source model is modified to include the effects of the gap and thickness-difference for the laser keyhole welding. The gap of the butt joint influences the welding efficiency such that the melting area decreases linearly with the gap. When the different plate thickness is used such as the tailored blank welding, melting areas of the thick and thin plates are predicted by introducing the thickness-difference factor. The calculated results using the modified heat source show reasonably good agreements with the experimental results.
DGEBA - MDA - SN - Hydroxyl Group System 의 합성 및 복합재료 제조 : 2 . 섬유강화 복합재료의 파괴에너지
이재영,심미자,김상욱 ( Jae Young Lee,Mi Ja Shim,Sang Wook Kim ) 한국공업화학회 1994 공업화학 Vol.5 No.4
유리섬유/탄소섬유/에폭시 수지 hybrid 복합재료의 파괴에너지를 파괴메카니즘 측면에서 연구하였다. 에폭시 수지 매트릭스는 DGEBA(diglycidyl ether of bisphenol A)-MDA(4,4`-methylene dianiline)-SN(succinonitrile)-HQ(hydroquinone)를 사용하였다. 섬유강화 복합재료의 파괴에너지를 연구한 결과, 유리섬유와 매트릭스의 계면에서는 post debond friction energy가 가장 크게 나타났으며, debonding energy와 pull-out energy는 비슷한 값을 나타내었다. 탄소섬유와 매트릭스의 계면에서 파괴가 일어나는 경우에는 pull-out energy가 가장 큰 영향을 나타내었다. The fracture energy of glass fiber/carbon fiber/epoxy resin hybrid composite system was investigated in the aspect of fracture mechanism. Epoxy resin matrix was DGEBA-MDA-SN-HQ system. On the interface of glass fiber and matrix, post debond friction energy provided a major contribution to the fracture energy, and debonding energy and pull-out energy were of the similar value. In the case of fracture on the interface of carbon fiber and matrix, pull-out energy was the major contributor.
Kissinger Equation 과 Fractional Life 법에 의한 DGEBA / MDA / MN 계와 DGEBA / MDA / MN / HQ 계의 경화반응 속도론
이재영,심미자,김상욱 ( Jae Young Lee,Mi Ja Shim,Sang Wook Kim ) 한국공업화학회 1994 공업화학 Vol.5 No.4
DGEBA/MDA/MN계와 이 계에 촉매로서 hydroquinone(HQ)를 첨가한 계의 경화반응 속도론을 Fractional life법 및 Kissinger equation에 의해 연구함으로써 HQ가 경화반응 속도에 미치는 영향을 연구하였다. 경화반응 온도가 증가함에 따라 반응속도는 증가하였고, 반응차수는 약간의 변화가 있을 뿐 경화온도에 따른 경향성은 없었다. 촉매로 HQ를 첨가한 계가 첨가하지 않은 계보다 반응속도는 크게 증가하였고, 활성화 에너지는 13% 감소하였다. 이는 HQ의 히드록 시기가 에폭사이드기, 아민기와 반응하여 전이상태를 형성함으로써 에폭사이드 고리를 쉽고 빠르게 개환시켜 주기 때문이다. Cure kinetics of DGEBA/MDA/MN system with and without HQ were studied by Fractional life method and Kissinger equation. And the effect of HQ as a catalyst was studied As cure temperature increased, the reaction rate increased and reaction order was almost constant. The activation energy of the system with HQ was lower about 13% and the reaction rate was higher than that of the system without HQ. It was because hydroxyl group of HQ formed a transition state with epoxide group and amine group and opened the epoxide ring easily and rapidly.
유천분지내 화강암류와 광상구의 관계에 대한 지화학적 연구
이재영,김상욱,김영기,고인석,장태우,Lee, Jae Yeong,Kim, Sang Wook,Kim, Young Ki,Koh, In Seok,Chang, Tae Woo 대한자원환경지질학회 1990 자원환경지질 Vol.23 No.2
There is clear difference in content of the major and trace elements between Masan granites of Cu province and Yucheon-Eonyang granites of Pb-Zn province in the Yucheon Basin: the former has low content in K(2.08%), Na(2.42%) and Rb (127ppm), and high content in Ca(3.75%), Mg(1.42%) and Sr(304ppm) whereas the latter has high content in K(3.56-3.60%), Na(3.05-3.06%) and Rb(144-161ppm), and low content in Ca(0.62-0.96), Mg(0.21-0.26%) and Sr(136-157ppm). Ore metals in granites also show slight difference between two areas: Masan granites have slightly higher Cu content(18ppm) than Yucheon-Eonyang granites(13, 14ppm), whereas Yucheon granite(29ppm) has slightly higher Pb content than Masan granites(25ppm). Thus, it may be possible to apply geochemical difference of the granites to distinguish whether a Cretaceous granite mass is related to copper or lead-zinc mineralization, and whether it belongs Cu-province or Pb-Zn province in the Yucheon Basin.
증착조건과 진공열처리 온도에 따른 ITO/PES 박막의 특성 연구
이재영,박지혜,김유성,천희곤,유용주,김대일,Lee, Jae-Young,Park, Ji-Hye,Kim, Yu-Sung,Chun, Hui-Gon,You, Yong-Zoo,Kim, Dae-Il 한국재료학회 2007 한국재료학회지 Vol.17 No.4
Transparent conducting indium tin oxide (ITO) films were deposited onto the Polyethersulfone (PES) substrate by using a magnetron sputter type negative metal ion source. In order to investigate the influence of cesium (Cs) partial pressure during deposition and annealing temperature on the optoelectrical properties of ITO/PES film the films were deposited under different Cs partial pressures and post deposition annealed under different annealing temperature from $100^{\circ}C$ to $170^{\circ}C$ for 20 min at $3\;{\times}\;10^{-1}$ Pa. Optoeleetrical properties of ITO films deposited without intentional substrate heating was influenced strongly by the Cs partial pressure and the Cs partial pressure of $1.5\;{\times}\;10^{-3}$ Pa was characterized as an optimal Cs flow condition. By increasing post-deposition vacuum annealing temperature both optical transmission in visible light region and electrical conductivity of ITO films were increased. Atomic force microscopy (AFM) micrographs showed that the surface roughness also varied with post-deposition vacuum annealing temperature.
시나리오 기반 하천-제내지 연계 통합수리해석에 의한 홍수위험도 산정
이재영,남명준,권현한,김기영,Lee, Jae Young,Nam, Myeong Jun,Kwon, Hyun Han,Kim, Ki Young 한국수자원학회 2016 한국수자원학회논문집 Vol.49 No.9
본 연구에서는 시나리오 기반의 홍수위험도를 산정하기 위해 하천-제내지 통합수리 해석모형이 적용되었다. 적용대상 유역으로 낙동강 및 금호강이 위치한 대구 성서공단 인근을 선정하여 하천홍수 발생으로 인한 시간별 범람수심 및 범람유속을 산정하였다. 하천-제내지 통합수리해석에 의한 2차원 범람해석은 100년/200년 빈도 신뢰구간 상한치(97.5%)에 의한 제방월류 시나리오와 100년/200년 빈도 신뢰구간 평균치(50%)에 의한 파제 시나리오로 구성하여 수행되었다. 또한 제내지 범람에 의한 위험도 산정을 위해 2차원 홍수범람도로부터 예측된 각 절점에 대한 최대 침수심 및 유속에 대한 정보를 이용하여 등급화를 실시하였다. 본 연구결과는 제방월류 및 파제에 따른 제내지의 비상대처계획(EAP) 수립에 정량적인 근거자료로 제시하는데 매우 유용할 것으로 사료된다. A coupled river-overland hydrodynamic model was applied to estimate flood risk by a scenario-based approach. The study area is Seongseo Industrial Complex in Daegu which is located near Nakdong river and Geumho river. Inundation depth and velocity at each time were calculated by applying a coupled 1D/2D hydrodynamic model to the target area of interest. The 2D inundation analysis for river and overland domain was performed with the scenario-based approach that there are levee overflow against 100/200 year high quantile (97.5%) design flood and levee break against 100/200 year normal quantile (50%) design flood. The level of flood risk was displayed for resident/industrial area using information about maximum depth and velocity of each node computed from the 2D inundation map. The research outcome would be very useful in establishing specified emergency action plans (EAP) in case of levee break and overflowing resulting from a flood.
이재영,김황희,신형진,김해도,권형중,전종찬,차상선,박찬기,Lee, Jae-young,Kim, Hwang-hee,Shin, Hyung-jin,Kim, Hae-do,Kwon, Hyung-joong,Jeon, Jong-chan,Cha, Sang-sun,Park, Chan-gi 한국농공학회 2018 한국농공학회논문집 Vol.60 No.3
Recently, the frequency and intensity of drought have been increasing due to the sudden abnormal climate in Korea. The occurrence of agricultural drought has been steadily increasing from 5 times in the 1980s to 2000s in 20 years, 6 times in the 10 years from 2000 to 2010, and 4 times in the recent period from 2011 to 2015. Therefore, this study analyzed the effect of water shortage caused by drought by improving the function of agricultural reservoir. The target area analyzed the data such as "Comprehensive Information System for Rural Water" operated by Korea Rural Community Corporation. As a result, we selected the target area as Wanju - gun, Jeollabuk - do in consideration of the rate of water storage compared with the normal 25 years, the completion year of the facility, the area of coverage per reservoir site and the low capacity. As a result of evaluating the improvement effect of agricultural facilities, it was analyzed that the irrigation area increased by about 25.7% when the water level was increased by 1m and the irrigation area increased by about 51.3% when the water level was increased by 2m. The results of the drought impact assessment after improving the function of the agricultural facilities were analyzed that it was effective to improve the function after more than 4m depth.