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Al-Mg-Si계 알루미늄 합금 판재 마찰교반접합부의 결정 방위 분포에 대한 용접후열처리의 영향
이광진,Lee, Kwang-Jin 대한용접접합학회 2009 대한용접·접합학회지 Vol.27 No.6
Friction stir welding (FSW) was carried out for Al-Mg-Si series aluminum alloys which are being used for automotive body structure. Consequently, Post weld heat treatment (PWHT) was applied to the friction stir welds to evaluate the effect of the paint baking process which is one of the automotive fabrication process on friction stir welded zone (FSWZ) in 443K for 1.2Ks. Grain structure and its crystal orientation distribution was measured about both the as welded specimens and the post weld heat treated specimens. An optical microscope (OM) and an field emission scanning electron microscope (FE-SEM) was used for observing the grain structure and measuring its crystal orientation distribution, respectively. Changes on the grain structure and its crystal orientation distribution were not detected. From the present results, it was confirmed that the paint baking process after FSW do not affect on the grain structure and its crystal orientation distribution of FSWZ. The comprehensive investigations will be performed for various automotive aluminum alloys manufactured by different processes, in the future.
이광진,김상혁,권의표,손규송,Lee, Kwang-Jin,Kim, Sang-Hyuk,Kwon, Eui-Pyo,Son, Kyu-Song 대한용접접합학회 2014 대한용접·접합학회지 Vol.32 No.2
Friction stir welding (FSW) was successfully performed about 900MPa grade Twinning Induced Plastisity (TWIP) steel. A PCBN tool with convex-type shoulder was applied. Optimal process conditions were deduced. Microstructure and mechanical properties such as hardness, tensile strength and impact absorbed energy were observed and evaluated, respectively. An optical microscope (OM) and a field emission scanning electron microscope (FE-SEM) was selected for observing the grain structure.
마찰교반용접(FSW) 및 마찰교반처리(FSP)의 최신 연구개발 동향
이광진,Lee, Kwang-Jin 대한용접접합학회 2013 대한용접·접합학회지 Vol.31 No.2
The latest research & development trend on friction stir welding and friction stir processing technologies presented in the international symposium, 'Friction Stir Welding & Processing VII'. Papers and presentations about high temperature materials such as advanced high strength steel, stainless steel and titanum alloy shoot up this year. Papers on modeling of metal flow and control of process parameters also increased. The FSP technologies for manufacturing of carbon materials reinforced metal matrix composites were reported, too.
A6061-T6/AZ31 이종금속 마찰교반접합부의 기계적 특성에 미치는 툴 삽입 위치의 영향
이광진,김상혁,Lee, Kwang-Jin,Kim, Sang-Hyuk 대한용접접합학회 2012 대한용접·접합학회지 Vol.30 No.5
Butt-joints of A6061-T6 and AZ31 plates were successfully manufactured by using a friction stir welding method. Off-set free joints and off-set joints were fabricated to investigate the effect of the tool plunge position on the mechanical properties of the joints. Hardness test, tensile test and charpy impact test was performed to evaluate the mechanical properties of the joints. Off-set condition resulted in increase of mechanical properties of the joints. The variation of the hardness distribution in the SZ was also stabilized in the off-set condition. Tensile strength of the off-set joint was about 85% against to that of the AZ31 base metal. Impact absorption energy by Charpy-Impact-Test of the off-set joint also increased by almost 2 times against to that of the AZ31 base metal.
On-line Screening HPLC-ABTS<sup>+</sup> Assay을 이용한 산청목으로부터 Salidroside의 분리 및 생물활성 분석
이광진,송나영,마진열,Lee, Kwang Jin,Song, Na-Young,Ma, Jin Yeul 한국생물공학회 2014 KSBB Journal Vol.29 No.2
Acer tegmentosum was a traditional Korean herbal medicine showing various pharmacological activities. In this work, A. tegmentosum were extracted with boiling water and then successively partitioned with dichloromethane, ethyl acetate, n-butyl alcohol (n-BuOH), and water. Salidoside, the target compound, was purified in n-BuOH phase using a chromatography method. For the analysis of salidoside, TLC and LC-MS were used as well as on-line screening $HPLC-ABTS^+$ assay with three different wavelength of 254, 280, and 320 nm. An amount of 1.34 g of salidoside were obtained in n-BuOH phase fromAcer tegmentosum was a traditional Korean herbal medicine showing various pharmacological activities. In this work, A. tegmentosum were extracted with boiling water and then successively partitioned with dichloromethane, ethyl acetate, n-butyl alcohol (n-BuOH), and water. Salidoside, the target compound, was purified in n-BuOH phase using a chromatography method. For the analysis of salidoside, TLC and LC-MS were used as well as online screening $HPLC-ABTS^+$ assay with three different wavelength of 254, 280, and 320 nm. An amount of 1.34 g of salidoside were obtained in n-BuOH phase from 3 kg of dry biomass. The on-line screening $HPLC-ABTS^+$ assay is rapid and efficient tool to search bioactivity from A. tegmentosum. 3 kg of dry biomass. The on-line screening $HPLC-ABTS^+$ assay is rapid and efficient tool to search bioactivity from A. tegmentosum.
이광진,김형자,Kwang-Jin, Lee,Hyung-Ja, Kim 한국기계가공학회 2004 한국기계가공학회지 Vol.3 No.3
The sub-surface stress field beneath the spur gear's contact surface in lubricated condition has been analysed. The surface pressure was obtained by the elasto-hydrodynamic lubrication analysis using the accurate geometric clearances around the contact region of the teeth. The sub-surface stress field was calculated by using the Love's rectangular patch solution. The analysis results show that the sub-surface stress distribution is quite dependent on the surface pressure distribution. The pattern of sub-surface stress field is similar to that of the external load. The depth where the maximum effective stress occurs is not proportional to the intensity of the external load.
최적 분석조건에 의한 강황으로부터 Curcuminoids의 고체상추출(SPE)
이광진(Lee, Kwang Jin),마진열(Ma, Jin Yeul),김영준(Kim, Young-Jun),김영식(Kim, Young-Shik) 한국산학기술학회 2012 한국산학기술학회논문지 Vol.13 No.10
강황은 다양한 약리활성을 가진 약초이다. 강황에 포함된 curcumin, demethoxycurcumin(DMC)과 bisdemethoxycurcumin(BDMC)을 침적과 초음파방법을 이용하여 추출하였다. 그리고 고체상추출(SPE)을 사용하여 추출효율을 확인 하였다. 추출액은 3가지 상업용 C<sub>18</sub> 역상 고성능 액체 크로마토그래피에 의해 이동상으로 물과 아세토나이트릴을 사용하여 일정용매법으로 동시분리·분석을 하였다. 유속은 1.0mL/min, 주입부피는 10μL, 컬럼오 븐 온도 40℃, 파장 425nm에서 수행되었다. 실험결과, RS tech column을 사용하고 물과 아세토나이트릴의 조성비 가 (50 : 50vol%)일 때 최적 조건을 얻을 수 있었다. 용매조성(물과 메탄올)에 따른 추출 수율에의 영향을 살펴본 결과 100% 메탄올에서 curcuminoids(추출시간 4h)가 가장 많이 추출되었고, 수용성 메탄올 조성보다 함량이 높았 다. 100% 물에 의해, 고체상추출은 curcuminoids의 추출함량(mAU×mim)이 침적과 초음파방법보다 24.5와 14.3배 높았다. 이상의 결과는 제약 및 기능성 소재로서의 응용 가능성을 나타내었다. Turmeric is a medicinal herb with various pharmacological activities. Curcumin, demethoxycurcumin(DMC) and bisdemethoxycurcumin(BDMC) were extracted from turmeric by dipping and ultrasonic wave method. And extraction efficiency was identified using solid phase extraction(SPE). The extracted sample were simultaneously separated and analyzed from three kinds of commercial C<sub>18</sub> reversed-phase high performance liquid chromatography using water and acetonitrile as mobile phase with isocratic elution mode. Flow rate 1.0mL/min, injection volume 10μL and column oven temperature 40℃ at 425nm wavelength has been conducted. From the experimental results, the optimum mobile phase composition of water/acetonitrile 50/50vol% using RS tech column. It is evident that the amount of curcuminoids extracted(extraction time 4h) by 100% MeOH was higher than any aqueous MeOH composition. Finally, in 100% water extraction, the amount(mAU×mim) of curcuminoids extracted by SPE was 14.3 and 24.5 times respectively higher than ultrasonic wave and dipping method. The shown results can be applied as sources for pharmaceuticals and functional material.