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윤기병,김동진,정헌생,Yun, Gi-Byeong,Kim, Dong-Jin,Jeong, Heon-Saeng 한국재료학회 1993 한국재료학회지 Vol.3 No.3
본 연구에서는 다공성 니켈재료의 원료분말로 활용될 수 있는 hollw 니켈금속분말 계조를 위한 니켈-흑연복합분말의 흑연코어 기화과정에 관하여 실험을 행하였다. 수증개-수소 혼합가스에 의한 복합분말중 흑연코어의 기화온도는 $800^{\circ}C$~$900^{\circ}C$였으며, 약 1시간의 기화반응에 의해 내부가 텅 빈 hollw니켈금속분말을 얻을 수 있었다. 흑연코어의 평균입도가 21$\mu\textrm{m}$인 82.2tw,% 니켈-17.87tw.5 흑연 복합분말로부터 제조된 hollw니켈금속분말을 100Kg/c$\textrm m^2$의 압력으로 압축, 성형한 성형체의 겉보기 기공도는 45%이었으며, 이성형체를 진공로에서 $1150^{\circ}C$ 의 온도로 1시간 소결하여 30%의 기공도와 소재내에 균질한 기공분포를 갖즌 소결체를 얻음으로써 다공성재료 제조시 hollow분말을 원료로 사용하여 재료 내의 기공에 관한 제반사항을 쉽게 조절할 수 있다는 가능성을 확인하였다. Abstract In this work. gasification of graphite cores from nickel-coated graphite composite powders was carried out to munufacture the hollow nickel metal powders which can be used as a raw materials for porous nickel metal strips. Graphite cores were gasified by $H_2O-H_2$ mixture gases at the temperature between $800^{\circ}C$ and $900^{\circ}C$ and nearly all removed from the composite powders within 1 hour. The hollow nickel metal powders prepared from 82.2wt. % Ni-17.8wt. % C composite powders which have the graphite cores of 21${\mu}$m average size were pressed and sintered at $1150^{\circ}C$ for 1 hour in vacuum furnace. The porosities of green and sintered compacts were 45% and 30%. respectively, and pores were distributed very homogeneously in the sintered compact. It was confirmed that pore distribution and porosity in porous materials can be easily controlled by using hollow powders as a raw materials.
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尹麒炳 現代醫學社 1968 現代醫學 Vol.9 No.1
The author studied the bacterial -contamination of -sewages in Taegu from September 1965 to ;December 1966 for the purpose of obtaining the rate of bacterial contamination in relation to " each district, season, pH and temperature. The results of the examination were summarized as follows: 1) The average number of the general bacterial count was approximately 200 million per ml. The most heavily contaminated area was Tong-Ku district. 2) The M.P.N. of E. coli was 5 million per 100 ml. in average. This -is an extremely high rate in comparison with its standard number of M.P.N. in - sewage. The highest rate was observed in Suh-Ku district. 3) Salmonella species were found in 29 cases (5.13%) out of 563 samples, most of them belonging to the group D (65%). Tong-Ku and Nam-Ku were higher in rate. 4) Shigella flexneri was found in 16 cases (2.84%) out of 563 samples. Both type 2 and 3 were found in higher" rate than other types, and type 5 was not detected at all. The highest rate was seen Nam-Ku district. 5) The relationship between the rate of bacterial contamnation and the season was as follows: Population of microorganism including E. coli and salmonella species increased in the spring, the summer and in the' fall and decreased in the winter. On the contrary shigella increased in the winter. 6) The relationship of the contamination rate with the temperature and pH was as follows: Population of microorganism including E. coli and salmonella increased in accordance W A the increasing degree of pH and temperature, while shigella increased in compliance' wit the decreasing degree of pH and temperatur 7) The detection rate of Salmonella in relation with the number of bacterial population includiaE E. coli showed that the rate was high in compliance with the number of bacteria, and that in cases of shigella the same tendency was observed as in Salmonella except cold season
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윤기병,Youn, Ki-Byoung 한국자원리싸이클링학회 2017 資源 리싸이클링 Vol.26 No.5
In-Bi-Sn alloy sheet has been used as a thermal fusible parts of secondary battery safety system. This study offers a simple process to make In-Bi-Sn alloy fusible parts. The process consists of two procedures, melting and sheeting by tape casting. 62.5 wt%-In 20.0 wt%-Bi 17.5 wt%-Sn (M.P. $92.4^{\circ}C$) alloy sheet obtained by tape casting was used as the thermal fusible sheet of thermal fuse system for mobile telephone. The performance test of the system was carried out in oil bath, and the fusible alloy sheet was melted and cut off at $95^{\circ}C$. This results confirmed the possibility that the alloy sheet obtained by tape casting can be usable as a thermal fusible parts of battery safety system. And this process can be applied as a simple process to recycle the In-Bi-Sn alloy scrap separated from the used thermal fuse system. 이차전지온도퓨즈시스템에 In-Bi-Sn계 저온가용합금 박판이 사용되고 있다. 본 연구에서는 온도퓨즈시스템에 사용될 수 있는 적절한 조성을 갖는 In-Bi-Sn계 합금을 용융하고 테이프캐스팅공정에 의하여 박판으로 제조하여 온도퓨즈용 저온가용합금 박판소재로 활용하는 가능성을 조사하였다. In-Bi-Sn계 용융합금은 기존의 박판제조공정보다 단순하고 생산성이 향상된 테이프캐스팅공정을 사용하여 박판화가 가능하다. 테이프캐스팅공정을 사용하여 얻은 62.5 wt%-In 20.0 wt%-Bi 17.5 wt%-Sn(융점 $92.4^{\circ}C$) 합금박판으로 휴대폰용 온도퓨즈시스템을 구성하여 $95^{\circ}C$에서 용락되는 기능이 나타남을 확인하였다. 이러한 공정은 폐In-Bi-Sn계 합금스크랩 처리에도 적용하여 합금조성과 박판두께를 적절히 조정하면 온도퓨즈시스템 가용합금 박판소재로 재활용할 수 있을 것으로 기대된다.
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電氣爐製鋼粉塵과 millscale 混合펠릿의 還元擧動에 관한 硏究
윤기병 한국자원리싸이클링학회 2000 資源 리싸이클링 Vol.9 No.6
전기로제강분진을 환원처리하여 철원으로 활용하는 경우, 매립폐기물 감소의 환경적 효과와 아울러 폐자원의 재자원화 효과가 기대된다. 본 연구에서는 제강공장에서 발생하는 millscale을 환원제와 함께 전기로제강분진에 혼합하고 회전상로에서 환원처리하여 Fe성분함량을 높이는 가능성을 조사, 검토하였다. millscale을 전기로제강분진에 혼합하여 처리함으로써 잔사 중의 Fe성분함량을 증가시킬 수 있었으며, 50 wt% millscale혼합 시 처리잔사 중의 $\boxDr$Fe성분함량은 85% 정도를 얻을 수 있었다. 회전상로에서 환원처리시 환원된 $\boxDr$Fe성분의 재산화가 일어나지 않도록 환원성분위기에서 가급적 빠른시간에 처리할 필요가 있으며 본 실험을 통하여 얻은 최적의 환원처리시간은 40분 정도이었다. 이때 잔사 중에 잔류하는 Zn및 Pb성분함량은 각각 3% 및 0.5%정도이었다. 환원성분위기에서 빠르게 처리된 경우의 처리잔사는 매립, 폐기 시 잔사 중에 함유된 금속성분들의 상당량이 용출되므로 별도의 사전처리 없이 매립, 폐기하여서는 않되며 전기로로 재투입하는 등 재활용하는 것이 바람직하다 Generally, the residues of EAF's dusts treated by reduction process at high temperature are disposed. If the residues can be recycled as iron sources of EAF by upgrading their iron contents, it can be expected to reduce the amounts of disposed wastes and the environmental impacts. Reduction of EAF's dusts mixed with millscale was carried out in rotary hearth furnace to upgrade iron contents of reduction residues. Dusts should be reduced rapidly to protect from reoxidation of reduced iron residue which can be reoxidized at high temperature. In our experimental conditions, optimum reduction time was about 40min. and iron contents of the residues were increased with increasing mixing ratio of millscale and upgrade to 85% at 50%wt mixing ratio. Zinc and lead contents in residues were about 3% and 0.5% respectively. The residues reduced rapidly must be recycled in EAF because heavy metal elements in the residues can be extracted easily and contaminate air and water.
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