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아조벤젠 분자(Disperse Red 1)를 포함한 측쇄형 고분자에서 광유도 복굴절의 실시간적 조사
신희득,주원제,오차환,송석호,김필수,한양규 한양대학교 자연과학연구소 2001 自然科學論文集 Vol.20 No.-
아조벤젠 그룹을 포함한 측쇄형 고분자 필름(PDR1)에서 광 유도된 이방성을 실시간적으로 조사하였다. 수평, 수직한 흡수율의 변화를 광 유도된 복굴절의 기록, 감쇠, 소거, 완화 과정에 따라 측정하여, 매질 내의 아조벤젠 분자의 정렬상태와 복굴절과의 관계를 광 이성화과정으로 설명하였다. 또한 기록빔의 세기를 따른 수직, 수평한 흡수율의 변화와 유도된 복굴절의 관계를 조사하였다. The photo-induced anisotropy for a polymeric film(PDR1) containing azobenzene group as side-chain was investigated dynamically. The change of absrobances with parallel and perpendicular components was measured in recording, decaying, erasing and relaxation processes of photo-induced birefringence, so the relation between the alignment of azobenzene groups and the birefringence was well explained according to the photo-isomerization. Also, the dependence of the photo-induced birefringence on intensity of recording beam was investigated with changes of both absorbance and birefringence.
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Synthesis and Photoisomerization Properties of Polynorbornenes with Azobenzene Chromophores
강석훈,신희득,오차환,최동훈,박기홍 대한화학회 2002 Bulletin of the Korean Chemical Society Vol.23 No.7
We successfully synthesized the addition-type polynorbonenes (PNB) exhibiting photochromic properties and excellent thermal stability. Three norbornene-based monomers with different azobenzene moiety (R=NO2, H, OCH3) were synthesized by transesterification method. The corresponding PNB copolymers were synthesized by transition metal-catalyzed addition polymerization method, and characterized by GPC, UV-Vis spectroscopy, NMR, and thermal analysis. For comparison of the photochromic properties depending on the rigidity of polymer backbone, we prepared the polymethylmethacrylate (PMMA) copolymer with the corresponding azobenzene moiety. We investigated the photoisomerization behavior by means of optical muitichannel analyzer with Xe lamp as well as real-time UV-Vis spectroscopy with high-pressure mercury lamp. Among three PNB copolymers, a polymer with azobenzene (R=H) was the most adaptable for observation of photoisomerization behavior. It was found that the rate of photoisomerization and relaxation depended on the structure of azobenzene chromophore, rather than that of polymer backbone.
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Fabrication method for ultra-long optical micro/nano-fibers
이동화,이광조,김진훈,박경득,이동진,김윤호,신희득 한국물리학회 2019 Current Applied Physics Vol.19 No.12
Nonlinear optical interactions can be enhanced dramatically by tight light-confinement and long interaction-length. Optical fiber tapers with micro/nano-thickness waists considerably increase light-matter interactions in or near their waists. Here, we propose and demonstrate a novel tapering method of fabricating uniform, low-loss, and ultra-long micro/nano fibers. The technique comprises three steps for conventional flame-brushing and pulling, recalibration, and one-directional pulling. Using the proposed method, two strands of tapered fibers are fabricated, having 0.82- μm/1.6-μm diameters, 220-mm/500-mm uniform lengths with<55-nm/66-nm diameter variances, and high transmittances of 90.2%/91.5%. A figure of merit indicating the nonlinear-optic efficiency is defined and used to compare the results obtained in this study with those for tapered fibers in references. The proposed tapering method will be very useful for the fabrication of tapered fiber devices exploiting nonlinear optic effects, including Brillouin scattering, Raman amplification, and other third-order nonlinearities for supercontinuum generation
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