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고상반응법을 이용한 Li<sub>2</sub>MnSiO<sub>4</sub> 합성
김지수,심중표,박경세,선호정,Kim, Ji-Su,Shim, Joong-Pyo,Park, Gyung-Se,Sun, Ho-Jung 한국전기전자재료학회 2012 전기전자재료학회논문지 Vol.25 No.5
Synthesis of $Li_2MnSiO_4$ was attempted by the conventional solid-state reaction method, and the phase formation behavior according to the change of the calcination condition was investigated. When the mixture of the three source materials, $Li_2O$, MnO and $SiO_2$ powders, were used for calcination in air, it was difficult to develop the $Li_2MnSiO_4$ phase because the oxidation number of $Mn^{2+}$ could not be maintained. Therefore, two-step calcination was applied: $Li_2SiO_3$ was made from $Li_2O$ and $SiO_2$ at the first step, and $Li_2MnSiO_4$ was synthesized from $Li_2SiO_3$ and MnO at the second step. It was easy to make $Li_2MnSiO_3$ from $Li_2O$ and $SiO_2$. $Li_2MnSiO_4$ single phase was developed by the calcination at $900^{\circ}C$ for 24 hr in Ar atmosphere as the oxidation of $Mn^{2+}$ was prevented. However, the $Li_2MnSiO_4$ was ${\gamma}-Li_2MnSiO_4$, one of the polymorph of $Li_2MnSiO_4$, which could not be used as the cathode materials in Li-ion batteries. By applying the additional low temperature annealing at $400^{\circ}C$, the single phase ${\beta}-Li_2MnSiO_4$ powder was synthesized successfully through the phase transition from ${\gamma}$ to ${\beta}$ phase.
한국 산업용 건물지붕 적용 PV에 의한 발전량 및 CO<sub>2</sub> 분석연구
김지수,이응직,황정하,Kim, Ji-Su,Lee, Eung-Jik,Hwang, Jung-Ha 한국태양에너지학회 2010 한국태양에너지학회 논문집 Vol.30 No.6
The purpose of this study is to provide foundational data for expansion of solar generation in building application, a clean energy, by introducing applicability of solar power generation system on roofs of industrial buildings and computing expected amounts of power and carbon dioxides reduction. As methodologies of this study, after reviewing 120,000 domestic factories to verify the BIPV feasibility for industrial building sthrough theoretical considerations of solar generation system, we calculated BIPV application methods and subsequent expected power generation quantity and carbon dioxide reductions through roof type analysis. we analyzed four cases of expected power generation amounts of solar batteries according to application methods, and when considering that the main type of roofs are slant roofs according to the investigation result about roof forms of domestic industrial complexes, we believe that the module angle of a slant roof around $17^{\circ}$(case3) is most suitable for the application. Finally, we came up with 517,944[TOE] as the corresponding petroleum tonnage based on this computed expected power generation amount and the amount of 1,214,836[$tCO_2$] carbon dioxide reductions by calculating them by energy sources.
천공분지에 기저를 둔 도서형 회전 근막 피부 피판을 이용한 압박궤양의 치료
김지수,김동훈,이동락,임준규,Kim, Ji-Su,Kim, Dong-Hoon,Lee, Dong-Lark,Lim, Jun-Kyu 대한미세수술학회 2007 Archives of reconstructive microsurgery Vol.16 No.1
The reconstruction of deep soft tissue defect such as pressure sore has difficult problems. Myocutaneous flaps have been used commonly as the best coverage method for pressure sore. But, they have several drawbacks such as sacrifice of functional muscle, high morbidity of the donor sites and bulkiness at the recipient site. The concepts of perforator flap has recently developed and widely used to overcome these disadvantages. Between March 2005 to July 2006, we have treated 9 patients who had pressure sore using perforator based fasciocutaneous island rotation flap. Preoperative unidirectional Doppler was used in all cases. Mean number of perforator vessels was 3.8 and flap sizes were from $7{\times}5\;cm$ to $14{\times}13\;cm$. Rotation angles of flap were from 90 degree to 180 degree. In all cases, donor sites were closed primarily. All flap survived completely and postoperative complications were wound dehiscence in 1 case, wound infection in 3 cases. The mean postoperative follow up period was 15.7 months and recurrence was not reported. We could decrease donor site morbidity and cover wound sites easily by using flap rotation and get robust blood supply without sacrifice of functional muscle. Fasciocutaneous perforator island rotation flap would be very useful for various pressure sore treatment.