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        Investigation of flexural strength and porosity of porous Si₃N₄ ceramics through orthogonal experimental design

        Juanli Yu,Jianmei Hou,Jian Zhang,Guanjun Qiao,Zhihao Jin,Hongjie Wang 한양대학교 세라믹연구소 2008 Journal of Ceramic Processing Research Vol.9 No.6

        Porous Si3N4 ceramics by a gel casting preparation route have received considerable attention because of their excellent performance. In this paper, orthogonal experimental design L16(45) was used to investigate the preparation of porous Si3N4 ceramics by a gelcasting technique. Three variables including solid loading, monomer content and the ratio of monomers were studied. Through range analysis and variance analysis, the results suggest that the ratio of monomers has a significant influence on both the flexural strength and porosity of Si3N4 sintered bodies. For the flexural strength of a Si3N4 sintered body, the order of significance levels was as follows: the ratio of monomers, solid loading and monomer content. For the porosity of a Si3N4 sintered body, the order of significance levels was as follows: the ratio of monomers, monomer content and solid loading. The experimental results suggest also that solid loading has an optimum value where the flexural strength can achieve a maximum value. Porous Si3N4 ceramics by a gel casting preparation route have received considerable attention because of their excellent performance. In this paper, orthogonal experimental design L16(45) was used to investigate the preparation of porous Si3N4 ceramics by a gelcasting technique. Three variables including solid loading, monomer content and the ratio of monomers were studied. Through range analysis and variance analysis, the results suggest that the ratio of monomers has a significant influence on both the flexural strength and porosity of Si3N4 sintered bodies. For the flexural strength of a Si3N4 sintered body, the order of significance levels was as follows: the ratio of monomers, solid loading and monomer content. For the porosity of a Si3N4 sintered body, the order of significance levels was as follows: the ratio of monomers, monomer content and solid loading. The experimental results suggest also that solid loading has an optimum value where the flexural strength can achieve a maximum value.

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        Mathematical Modeling of Drying Kinetics for Pulp Sheet Based on Fick’s Second Law of Diffusion

        Lingbo Kong,Xing Yang,Zhihao Hou,Jixian DONG 한국펄프·종이공학회 2020 펄프.종이기술 Vol.52 No.2

        In this study, we investigated the drying characteristics for pulp sheet at different hot air temperature (80, 90, and 100℃). The drying kinetics were modeled using one- to five-term solutions of Fick’s second law of diffusion at different drying conditions. It was found that these models underestimated the initial drying stages and overestimated the final drying stages. Meanwhile, the values of the diffusion coefficient tended to stabilize when the series terms more than three. In order to improve the accuracy of the mathematical models, the modified one- to three-term models were also used to describe the drying kinetics. The results showed that modeling data was agreed with the experiment data better than the series solution models based on Fick’s second law of diffusion. Besides, the accuracy improved dramatically as the terms of the model increased. The minimum diffusion coefficient was 0.996 for the modified three-term model. It was concluded that the modified model could simulate the pulp sheet drying process under the conditions studied.

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