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GUANGLIANG CHEN,FEI XUE,ZHILI CHEN,XIAOLEI SI,JUN HUANG,XU ZHENG,SYLVAIN MASSEY 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2014 NANO Vol.9 No.3
In this paper, homogenous gold nanoparticles (AuNPs) with a high density and a narrow sizedistribution were successfully fabricated on titanate nanowires (TNWs) sca®olds in the absenceof organic capping agents. An ameliorated low-temperature hydrothermal method was used toprepare the TNWs sca®olds like bird's nest on the Ti substrate, and the nanowires diameter wasabout 30 – 80nm. Then, AuNPs were synthesized on the TNWs sca®olds with a deposition –precipitation urea (DPU) method. The TEM and XRD measurements indicated that well-crys-tallized face-centered cubic (fcc) AuNPs were homogeneously dispersed on TNWs, and AuNPswith average sizes of 2.7 nm and 4 nm were obtained, respectively for the theoretical gold loading5 wt.% and 8 wt.%. Inspiringly, the 8%-AuNPs/TNWs catalyst could reduce 4-nitrophenol (4-NP) to 4-aminophenol (4-AP) within 210 s, and exhibited better catalytic reduction performancethan that of 5%-AuNPs/TNWs.