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Purification of naphthalene from eutectic mixture by continuous column crystallization
Zhengming Yi,Qunsheng Li,Xufeng Sun,Minggao Su 한국화학공학회 2010 Korean Journal of Chemical Engineering Vol.27 No.2
To obtain highly purified naphthalene, a column crystallizer was employed and operated in the continuous multistage countercurrent fractional mode. The principles and characteristics of the process are introduced. A large amount of experimental work has been done on the crystallization process in a D=50 mm×1,350 mm column. The effects of operation conditions including the composition of feed, reflux ratio, stirring speed and the bed height of crystal on crystallization were systematically studied. The experiments showed that over 99.0% of the purity of product can be easily achieved in such conditions: feed composition among w=85.462-95.894%, reflux ratio among 1.42-4.04,the crystal bed height among 400-900 mm. The purity of product even reaches 99.996% in experiment.
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Phenol removal via activated carbon from co-pyrolysis of waste coal tar pitch and vinasse
Ming Gao,Xiaona Wang,Changlei Xia,Na Song,Yuhui Ma,Qunhui Wang,Tianxue Yang,Shengbo Ge,Chuanfu Wu,Su Shiung Lam 한국화학공학회 2021 Korean Journal of Chemical Engineering Vol.38 No.1
The behavior and characteristics of phenol adsorption by activated carbon produced from co-pyrolysis of coal tar pitch and vinasse were investigated. Coal tar pitch and vinasse (mass ratio of 1 : 3) were firstly co-pyrolyzed and carbonated at 400 oC for 2 h. The carbonized material produced was then soaked with saturated KOH solution and activated at 800 oC for 1 h to form activated carbon. Results from the phenol wastewater adsorption experiments suggest that pseudo-second-order kinetics and the Weber-Morris model could reflect the time-dependent adsorption behavior of phenol wastewater by the activated carbon, revealing that internal diffusion represents the rate-limiting procedure and dominant process to control the adsorption rate in the early stage of the adsorption. Monolayer adsorption played the key role during the phenol adsorption. The adsorption was an endothermic reaction in temperature ranging from 15 oC to 35 oC, indicating that the adsorption speed could be stimulated by the increasing temperature. This study establishes a theoretical foundation for the usage and the potential application of the activated carbon derived from coal tar pitch and vinasse in wastewater treatment.
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