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- 저자 : M.A. Cortes-Jácome (검색결과 1 건)
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WOx nanoclusters highly dispersed on titania nanofibers
C. Angeles-Chavez,M.A. Cortes-Jácome,J.A. Toledo-Antonio 한양대학교 세라믹연구소 2008 Journal of Ceramic Processing Research Vol.9 No.5
WOx-TiO2 catalysts with different W contents on titanium oxide nanofibers were prepared by impregnation of (NH4)2WO4 aqueous solution and annealed in air at 400 oC. X-ray diffraction (XRD), high resolution transmission electron microscopy (HRTEM), high angle annular dark field scanning transmission electron microscopy (HAADF-STEM) and Raman spectroscopy were used for chemical and structural characterization. The results revealed that the support consisted of β-titanium oxide nanofibers with WOx species highly dispersed on the nanofibers saturating the surface at a concentration around 30 wt%. With an increase in the W concentration to 40 and 50 wt%, a crystalline WO3 phase segregates from the support, growing as large WO3 crystallites, whereas the support remains homogeneously decorated by WOx nanoclusters with dimensions around 1.0 nm. The W atoms remained octahedrally coordinated with a W = O Raman vibrating band at 974 cm−1. WOx-TiO2 catalysts with different W contents on titanium oxide nanofibers were prepared by impregnation of (NH4)2WO4 aqueous solution and annealed in air at 400 oC. X-ray diffraction (XRD), high resolution transmission electron microscopy (HRTEM), high angle annular dark field scanning transmission electron microscopy (HAADF-STEM) and Raman spectroscopy were used for chemical and structural characterization. The results revealed that the support consisted of β-titanium oxide nanofibers with WOx species highly dispersed on the nanofibers saturating the surface at a concentration around 30 wt%. With an increase in the W concentration to 40 and 50 wt%, a crystalline WO3 phase segregates from the support, growing as large WO3 crystallites, whereas the support remains homogeneously decorated by WOx nanoclusters with dimensions around 1.0 nm. The W atoms remained octahedrally coordinated with a W = O Raman vibrating band at 974 cm−1.
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