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Qiaoran Zhang,Zhiwei Li,Xiaohong Li,Laigui Yu,Zhijun Zhang,Zhishen Wu 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2019 NANO Vol.14 No.5
Boron nitride nanosheet (BNNS) decorated with cobalt ferrite nanoparticle (CFN) to afford CFN-BNNS nanohybrid was prepared via a simple hydrothermal route and was well characterized. Subsequently, the as-prepared CFN-BNNS nanohybrid was incorporated into epoxy resin (EP) with the introduction of a weak rotary magnetic field to achieve order orientation, in order to reduce the fire risk and toxic hazards using enhanced shielding effect of BNNS upon combustion. Findings demonstrate that the CFN-BNNS nanohybrid is composed of CFN nanoparticle uniformly dispersed on BNNS surface. Thermal analysis and cone calorimeter data show that the CFN-BNNS nanofiller among EP matrix contributes to improving the char residues and mechanical properties of EP and reducing its fire risk as well as toxic hazards, especially the ordered one is advantageous over the disordered one in reducing the fire risk and toxic hazard. This is because, on the one hand, the orderly aligned BNNS as the physical barrier can more effectively prevent the transfer and diffusion of oxygen and heat. On the other hand, CFN can catalyze the degradation of EP to afford excessive chars on polymer surface; and it is also liable to decomposition during combustion, thereby generating ferrite species to promote EP degradation as well as cobalt species to enhance the oxidation of CO.
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Mengmeng Zhang,Yamin Cheng,Zhiwei Li,Xiaohong Li,Laigui Yu,Zhijun Zhang 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2019 NANO Vol.15 No.01
An inorganic–organic nanohybrid flame retardant, HNT@CS@Fe3O4, is prepared by Halloysite nanotubes (HNT) as nanotemplate, chitosan (CS) as char-forming agent and ferroferric oxide (Fe3O4) playing in a catalytic role, aiming to endow enhanced flame-retardant performance of its nanohybrid. Results show that HNT@CS@Fe3O4 nanohybrids have a corn-like structure and can significantly improve the flame retardancy and thermal stability of epoxy resin (EP). Especially, the initial thermal degradation temperature of EP/HNT@CS@Fe3O4 is significantly improved by 24 ℃ relative to pure EP, and the residual carbon yield under air atmosphere is 8.8 wt.%, which is significantly higher than other EP composites, indicating a higher thermal stability is offered by the as-prepared nanohybrid. The limiting oxygen index of EP/10HNT@CS@Fe3O4 is 31.3%, which is 10.2% higher than that of pure EP. Meanwhile, the HNT@CS@Fe3O4 nanofiller reduces the peak heat release rate, CO production and peak smoke production release of EP nanocomposite by 32.0%, 44.0% and 33.0% in a cone calorimeter test, respectively. This is because the HNT-based composite can form a three-dimensional network structure into the EP matrix to inhibit heat release and diffusion of flammable moieties upon burning of EP. In the meantime, the incorporated Fe3O4 nanoparticle can in situ catalyze the charring of CS and EP matrix on the surface of HNT during the combustion process, which also contributes to the significantly increased fire safety of EP.
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