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        Preparing cuprous oxide nanomaterials by electrochemical method for non-enzymatic glucose biosensor

        Nguyen, Thu-Thuy,Huy, Bui The,Hwang, Seo-Young,Vuong, Nguyen Minh,Pham, Quoc-Thai,Nghia, Nguyen Ngoc,Kirtland, Aaron,Lee, Yong-Ill IOP 2018 Nanotechnology Vol.29 No.20

        <P>Cuprous oxide (Cu<SUB>2</SUB>O) nanostructure has been synthesized using an electrochemical method with a two-electrode system. Cu foils were used as electrodes and NH<SUB>2</SUB>(OH) was utilized as the reducing agent. The effects of pH and applied voltages on the morphology of the product were investigated. The morphology and optical properties of Cu<SUB>2</SUB>O particles were characterized using scanning electron microscopy, x-ray diffraction, and diffuse reflectance spectra. The synthesized Cu<SUB>2</SUB>O nanostructures that formed in the vicinity of the anode at 2 V and pH?=?11 showed high uniform distribution, small size, and good electrochemical sensing. These Cu<SUB>2</SUB>O nanoparticles were coated on an Indium tin oxide substrate and applied to detect non-enzyme glucose as excellent biosensors. The non-enzyme glucose biosensors exhibited good performance with high response, good selectivity, wide linear detection range, and a low detection limit at 0.4 <I>μ</I>M. Synthesized Cu<SUB>2</SUB>O nanostructures are potential materials for a non-enzyme glucose biosensor.</P>

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