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Junhong Chen,Mingwei Yan, Yong Li,Zhijian Li,Jindong Su,Bin Li,Jialin Sun 한양대학교 세라믹연구소 2016 Journal of Ceramic Processing Research Vol.17 No.5
Periclase-hercynite bricks were prepared from fused or reaction-sintered hercynite. The microstructure of the obtained brickswas studied and their thermal conductivity in the simulated on-site condition was tested. The results show that the mutualdiffusion of Fe or Al from hercynite and Mg from periclase forms more pores in the material. Compared with the brickprepared from fused hercynite, the brick from reaction-sintered hercynite has smaller pore size. The thermal conductivitysimulation test of the two bricks at 1550 oC shows that the cold end temperature of the brick synthesized from the reactionsinteredhercynite is 40 oC lower than that of the brick from the fused hercynite. Thus, in consideration of reducing the shelltemperature of the cement rotary kilns, the reaction-sintered hercynite is more favorable for the production of periclasehercynitebricks.
Structure of hercynite prepared with existence of metal Fe
Junhong Chen,Dongfang Liu,Mingwei Yan, Yong Li,Jindong Su,Bin Li,Jialin Sun 한양대학교 세라믹연구소 2016 Journal of Ceramic Processing Research Vol.17 No.12
In this work, raw materials analytically pure Al2O3 and analytically pure Fe2O3 were mixed in FeO: Al2O3 molar ratio of 1 : 1and pressed into specimens. The specimens were embedded in analytically pure metal Fe powders and fired slowly to 1650 oCin air atmosphere, and then soaked at 1650 oC for 5 hrs. The fired specimens were investigated by XRD, SEM, and EDS. Theresults show that the specimen synthesized at high temperatures in melting Fe is composed of hercynite and wüstite (FenO(n ≤ 1)); FenO disperses in hercynite; hercynite crystals develop well and are mostly perfect octahedron with grain size around50μm. The hercynite has Fe/Al ratio smaller than 1/2, which is non-stoichimetric. With the existence of melting Fe, althoughthe raw materials are theoretically batched according to FeO·Al2O3, FenO is still excess, so the hercynite obtained is Al-rich.