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Research on Rapid Detection Method of Dry Matter Content in Raw Milk Based on Mid-infrared Spectrum
Xiaoming Li,Guicheng Huo,Yan Wang,Qingming Kong,Hongmin Sun 보안공학연구지원센터 2016 International Journal of u- and e- Service, Scienc Vol.9 No.9
This paper takes raw milk as research object, and using mid-infrared spectrum analysis method rapidly tests dry matter in raw milk through establishing quantitative analysis model. First of all, researchers collect 84 kinds of raw milk which is different areas and varieties in Heilongjiang province, and classify 84 samples into calibration sets and validation sets by standard chemical testing and spectral scanning on raw milk, and calibration sets contain 64 samples, and validation sets contain 20 samples. Then, respectively selecting SPA and GA characteristic wavelength after treating by smoothing denoising method which window size is 11 points, and establishing PLS model and model demonstration. Eventually, researchers draw the conclusion that SPA wavelength selection method which value of m_max is 10 and GA wavelength selection method which value of Evaluat is 10d can effectively improve validation set model precision, but precision of the latter is higher and characteristic wavelength point reduces from 352 to 10, The calibrating determination coefficient R2 of model is 0.8092155, root mean square error (RMSEC ) is 0.1206172. Validation set determination coefficient R2 is 0.8620867, the root mean square error (RMSEC) is 0.0950656, and relative standard deviation RSD<3%. These prove that the method for rapid testing of raw milk components is feasible.
Research on Rapid Detection Method of Protein and Fat in Raw Milk Based on Mid-infrared Spectrum
Xiaoming Li,Guicheng Huo,Yan Wang,Hongmin Sun,Qingming Kong 보안공학연구지원센터 2016 International Journal of Multimedia and Ubiquitous Vol.11 No.10
In this paper raw milk was taken as the research object, using mid-infrared spectrum analysis method rapidly tests protein and fat content in raw milk through establishing quantitative analysis model. First of all, researchers collect 84 kinds of raw milk which is different areas and varieties in Heilongjiang province, and classify 84 samples into calibration sets and validation sets by standard chemical testing and spectral scanning on protein and fat, and calibration sets contain 64 samples, and validation sets contain 20 samples. Then, denoising by second derivative method which window size is 17 points, and selecting method by comparing SPA and GA characteristic wavelength respectively, and establishing PLS model and model demonstration. Eventually, researchers draw the conclusion that SPA wavelength selection method which value of m_max is 10 and GA wavelength selection method which value of Evaluat is 10d can effectively improve validation set model precision, but precision of the former is higher and characteristic wavelength is least, and its characteristic wavelength point reduces from 220 to 4, R2 of protein model validation set is 0.8010929, RMSEP is 0.0207505, R2 of fat model validation set is 0.91007989, RMSEP is 0.045329, relative standard deviation RSD<3%. These prove that the method for rapid testing of raw milk components is feasible.