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        Carbonaceous catalysts from orange pulp for limonene oxidation

        Wróblewska Agnieszka,Serafin Jarosław,Gawarecka Alicja,Miądlicki Piotr,Urbaś Karolina,Koren Zvi C.,Llorca Jordi,Michalkiewicz Beata 한국탄소학회 2020 Carbon Letters Vol.30 No.2

        The possibility of orange pulp utilization for nanoporous carbons production was investigated. Moreover, processing the obtained materials as limonene oxidation catalysts was studied as well. Limonene was separated from orange pulp obtained from fragmented orange peels—the waste from industrial fruits processing—by means of simple distillation. After the sepa�ration of limonene from the biomass, the dried orange pulp was converted to three types of nanoporous carbon catalysts: without activating agent, with NaOH, and with KOH. The catalysts were characterized by XRD, SEM, EDX, AFM, and sorption of N2 methods. The activities of the obtained catalysts were tested in the oxidation of limonene to perillyl alcohol (the main product), carveol, carvone, and 1,2-epoxylimonene and its diol. In the oxidation processes, hydrogen peroxide was used as the oxidizing agent. This work has shown for the frst time that nanoporous carbons obtained from orange pulp waste, after separation of limonene, are active catalysts for limonene oxidation to industrially important value-added products.

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