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RISS 인기검색어
- 검색키워드
- 저자 : Danda Srinivas Rao (검색결과 2 건)
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Sandeep Panda,Srabani Mishra,Danda Srinivas Rao,Nilotpala Pradhan,Umaballava Mohapatra,Shivakumar Angadi,Barada Kanta Mishra 한국화학공학회 2015 Korean Journal of Chemical Engineering Vol.32 No.4
Copper slag was subjected to in-depth mineralogical characterization by integrated instrumental techniquesand evaluated for the efficacy of physical beneficiation and mixed meso-acidophilic bioleaching tests towardsrecovery of copper. Point-to-point mineral chemistry of the copper slag is discussed in detail to give better insight intothe association of copper in slag. Characterization studies of the representative sample revealed the presence of fayaliteand magnetite along with metallic copper disseminated within the iron and silicate phases. Physical beneficiation of thefeed slag (~0.6% Cu) in a 2 L working volume flotation cell using sodium isopropyl xanthate resulted in Cu beneficiationup to 2-4% and final recovery within 42-46%. On the other hand, a mixed meso-acidophilic bacterial consortiumcomprised of a group of iron and/or sulfur oxidizing bacteria resulted in enhanced recovery of Cu (~92-96%) from theslag sample. SEM characterization of the bioleached slag residue also showed massive coagulated texture with severeweathered structures. FE-SEM elemental mapping with EDS analysis indicated that the bioleached residues were devoidof copper.
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Studies on removal of lead ions from aqueous solutions using iron ore slimes as adsorbent
Laxmipriya Panda,Bisweswar Das,Danda Srinivas Rao 한국화학공학회 2011 Korean Journal of Chemical Engineering Vol.28 No.10
Iron ore slimes, a waste material generated during iron ore mining have been employed for the removal of lead ions from aqueous solutions by a batch adsorption technique. The slime sample contains 45.8% Fe, 13.6% SiO_2,and 13.9% Al_2O_3. It is characterized by X-ray diffraction (XRD) and optical microscopy to determine the presence of different phases such as hematite, goethite, limonite, quartz and kaolinite. It is assumed that the adsorption of lead ions is mainly due to the presence of pores and cavities in goethite mineral. The FTIR studies showed the presence of Si-OH and Fe-OH sites responsible for adsorption. Furthermore, the point of zero charge (pzc) of iron ore slime is shifted from 6.2 to 5.8 due to the adsorption of lead ions. Batch adsorption experiments have been conducted to study the sorption behavior of lead ions on iron ore slime. The effects of agitation time, concentration of lead ions, adsorbent doses, solution pH, other metal ions and temperature on the amount of lead ions adsorbed have been investigated. Lead ion adsorption is fast, and equilibrium could be achieved within 15 minutes of time. The adsorption increased with increase in temperature suggesting an endothermic adsorption. Under the conditions, it is possible to remove 95%lead from an aqueous solution bearing ~20 mg/l at pH~5.1. The equilibrium adsorption isotherm data fitted very well to both Langmuir and Freundlich adsorption models.
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