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- 저자 : Binbin Chang (검색결과 2 건)
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Cost-Effective Fabrication of Biomorphic Mesoporous Ni-NiO Microtube for Pseudocapacitors
Binbin Chang,Hang Yin,Zhengyan Gu,Zhikun Li,Baocheng Yang 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2016 NANO Vol.11 No.11
In this paper, a biomorphic mesoporous Ni-NiO microtube was successfully prepared by a facile and cost-effective synthesis strategy using cotton as a biotemplate. The morphology and textural characterization of as-obtained Ni-NiO materials were analyzed by X-ray diffraction patterns, scanning electron microscopy and nitrogen adsorption–desorption technology. The results suggested the as-prepared Ni-NiO samples owned uniform micro-tubular morphology and prominent mesoporous structure. Meanwhile, the effect of annealing temperature on morphology and porosity of Ni-NiO was also investigated. The optimal sample, Ni-NiO-4, exhibited a uniform microtube morphology with an ideal mesoporous structure of a high surface area (15.8 m2 g-1) and suitable mesopore size (9.28 nm). Furthermore, these as-obtained Ni-NiO materials showed enhanced electrochemical property as electrodes for pseudocapacitors. Especially, the Ni-NiO-4 electrode displayed the outstanding capacitive performance, including a high specific capacitance of 98.7 F g-1 at 0.5 A g-1 and satisfactory rate capacity. More importantly, Ni-NiO-4 electrode owned an excellently long-term cycling stability.
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Qiu, Jijun,Weng, Binbin,Zhao, Lihua,Chang, Caleb,Shi, Zhisheng,Li, Xiaomin,Kim, Hyung-Kook,Hwang, Yoon-Hwae Hindawi Limited 2014 Journal of nanomaterials Vol.2014 No.-
<P>Flower-like bundles of ZnO nanosheets have been prepared by using preheating hydrothermal process without any surfactants. The flower-like bundles consist of many thin and uniform hexagonal-structured ZnO nanosheets, with a thickness of 50 nm. The selected area electronic diffraction (SAED) and high-resolution transmission electron microscope (HRTEM) images indicate that the ZnO nanosheets are single crystal in nature. The growth mechanism of the flower-like bundles of ZnO nanosheets is discussed based on the morphology evolution with growth times and reaction conditions. It is believed that the formation of flower-like bundles of ZnO nanosheets is related to the shielding effect of OH<SUP>−</SUP>ions and the self-assembly process, which is dominated by a preheating time. Room temperature photoluminescence spectra results show that the annealing atmosphere strongly affects the visible emission band, which is sensitive to intrinsic and surface defects, especially oxygen interstitials, in flower-like bundles of ZnO nanosheets.</P>
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